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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
(±)-驴食草酚
合成路线
（共 9 条）
1029608-33-0
→
反应条件
56701-24-7
(±)-驴食草酚
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate 24 h;
参考文献
Gharpure, Santosh J.; Sathiyanarayanan; Jonnalagadda, Prasad
Tetrahedron Letters, 2008 , vol. 49, # 18 p. 2974 - 2978
1322728-39-1
→
反应条件
56701-24-7
(±)-驴食草酚
反应条件
palladium 10 on activated carbon; hydrogen in ethyl acetate P=1800.18 Torr;
参考文献
Luniwal, Amarjit; Erhardt, Paul W.
Synlett, 2011 , # 11 p. 1605 - 1607
412339-25-4
→
反应条件
56701-24-7
(±)-驴食草酚
反应条件
1: potassium carbonate / acetone / Inert atmosphere; Reflux 2: acetonitrile / Inert atmosphere 3: potassium tert-butylate / methanol / Inert atmosphere; Reflux 4: palladium 10 on activated carbon; hydrogen / ethyl acetate / 1800.18 Torr View Scheme
参考文献
Luniwal, Amarjit; Erhardt, Paul W.
Synlett, 2011 , # 11 p. 1605 - 1607
1322728-38-0
→
反应条件
56701-24-7
(±)-驴食草酚
反应条件
1: acetonitrile / Inert atmosphere 2: potassium tert-butylate / methanol / Inert atmosphere; Reflux 3: palladium 10 on activated carbon; hydrogen / ethyl acetate / 1800.18 Torr View Scheme
参考文献
Luniwal, Amarjit; Erhardt, Paul W.
Synlett, 2011 , # 11 p. 1605 - 1607
1322728-37-9
→
反应条件
56701-24-7
(±)-驴食草酚
反应条件
1: potassium carbonate / acetone / Inert atmosphere; Reflux 2: acetonitrile / Inert atmosphere 3: potassium tert-butylate / methanol / Inert atmosphere; Reflux 4: palladium 10 on activated carbon; hydrogen / ethyl acetate / 1800.18 Torr View Scheme
参考文献
Luniwal, Amarjit; Erhardt, Paul W.
Synlett, 2011 , # 11 p. 1605 - 1607
4136-21-4
2-羟基-1-(4-甲氧基苯基)-1-乙酮
→
反应条件
56701-24-7
(±)-驴食草酚
反应条件
1: potassium carbonate / acetonitrile / 24 h / Reflux 2: iodine; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) / methanol; dichloromethane / 20 h 3: potassium carbonate / acetone / Inert atmosphere; Reflux 4: acetonitrile / Inert atmosphere 5: potassium tert-butylate / methanol / Inert atmosphere; Reflux 6: palladium 10 on activated carbon; hydrogen / ethyl acetate / 1800.18 Torr View Scheme
参考文献
Luniwal, Amarjit; Erhardt, Paul W.
Synlett, 2011 , # 11 p. 1605 - 1607
52249-86-2
1-[2-(苄氧基)-4-甲氧基苯基]-1-乙酮
→
反应条件
56701-24-7
(±)-驴食草酚
反应条件
1: iodine; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) / methanol; dichloromethane / 20 h 2: potassium carbonate / acetone / Inert atmosphere; Reflux 3: acetonitrile / Inert atmosphere 4: potassium tert-butylate / methanol / Inert atmosphere; Reflux 5: palladium 10 on activated carbon; hydrogen / ethyl acetate / 1800.18 Torr View Scheme
参考文献
Luniwal, Amarjit; Erhardt, Paul W.
Synlett, 2011 , # 11 p. 1605 - 1607
95-01-2
2,4-二羟基苯甲醛
→
反应条件
56701-24-7
(±)-驴食草酚
反应条件
1: potassium hydrogencarbonate / acetonitrile / 15 h / Reflux 2: sodium tetrahydroborate / ethanol / 11 h / 0 - 20 °C 3: potassium carbonate / acetone / Inert atmosphere; Reflux 4: acetonitrile / Inert atmosphere 5: potassium tert-butylate / methanol / Inert atmosphere; Reflux 6: palladium 10 on activated carbon; hydrogen / ethyl acetate / 1800.18 Torr View Scheme
参考文献
Luniwal, Amarjit; Erhardt, Paul W.
Synlett, 2011 , # 11 p. 1605 - 1607
52085-14-0
4-苯甲氧基-2-羟基苯甲醛
→
反应条件
56701-24-7
(±)-驴食草酚
反应条件
1: sodium tetrahydroborate / ethanol / 11 h / 0 - 20 °C 2: potassium carbonate / acetone / Inert atmosphere; Reflux 3: acetonitrile / Inert atmosphere 4: potassium tert-butylate / methanol / Inert atmosphere; Reflux 5: palladium 10 on activated carbon; hydrogen / ethyl acetate / 1800.18 Torr View Scheme
参考文献
Luniwal, Amarjit; Erhardt, Paul W.
Synlett, 2011 , # 11 p. 1605 - 1607
