双-[3-(三乙氧基硅)丙基]-二硫化物合成路线 （共 27 条）
反应条件
sodium hydrogen sulphate; sodium hydrogensulfide; tetrabutylammomium bromide in water T=75°C; 5.63333 h;
参考文献
US6680398 B1, ;
Page column 10-11 ;
反应条件
sodium sulfide; sodium hydrogensulfide; tetrabutylammomium bromide in water T=70 - 82°C; 3 h;
参考文献
US6680398 B1, ;
Page column 8 ;
反应条件
sodium sulfide; sodium polysulfide in ethanol T=78°C; Product distribution / selectivity;
参考文献
Frings, Albert; Janssens, Louis; Lotter, Stefan; Deschler, Ulrich; Alig, Alfred
Patent: US2007/66841 A1, 2007 ;
Location in patent: Page/Page column 4 ;
反应条件
NaHS monohydrate; sodium carbonate; sulfur; sodium hydroxide in ethanol; water T=55 - 80°C; Product distribution / selectivity;
参考文献
US2010/29971 A1, ;
Page/Page column 9-10 ;
反应条件
sodium sulfide; tetrabutylammomium bromide; sulfur in water T=80 - 90°C; 5.66667 h; Product distribution / selectivity;
参考文献
US2006/106240 A1, ;
Page/Page column 4 ;
反应条件
NaHS monohydrate; sodium carbonate; sulfur; sodium hydroxide in ethanol; water T=65 - 75°C; Product distribution / selectivity;
参考文献
US2010/29971 A1, ;
Page/Page column 10 ;
反应条件
1: With sulfur in toluene T=80°C; 2: With tetrabutylammomium bromide; sulfur in water; toluene T=80 - 85°C; 5.58333 h; Product distribution / selectivity;
参考文献
US2006/106240 A1, ;
Page/Page column 4-5 ;
反应条件
1: With sulfur T=80°C; 2: With Na2S3; tetrabutylammomium bromide in water T=80 - 90°C; 3.66667 h; Product distribution / selectivity;
参考文献
US2006/106240 A1, ;
Page/Page column 4 ;
