[[P-(2-甲氧基乙基)苯氧基]甲基]环氧乙烷合成路线 （共 27 条）
反应条件
sodium hydroxide in water T=40 - 45°C; 3 - 5 h;
参考文献
IPCA LABORATORIES LIMITED
Patent: WO2005/46568 A2, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
1: H2; AcOH / Pd/C 2: 90 percent / aq. NaOH View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 14, # 1 p. 191 - 194
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 14, # 1 p. 191 - 194
反应条件
1: methanol 2: H2; AcOH / Pd/C 3: 90 percent / aq. NaOH View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 14, # 1 p. 191 - 194
反应条件
1: CuBr2 / ethyl acetate 2: methanol 3: H2; AcOH / Pd/C 4: 90 percent / aq. NaOH View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 14, # 1 p. 191 - 194
反应条件
sodium methylate in methanol T=50 - 60°C; 0.5 h;
参考文献
Gurjar, M.K.; Joshi, Shreerang V; Sastry, B.S.; Rao, A V Rama
Synthetic Communications, 1990 , vol. 20, # 22 p. 3489 - 3496
反应条件
1: 90 percent / methanol / 24 h / Ambient temperature 2: 96 percent / H2 / 10percent Pd/C / ethanol / 4 h / 2327.2 Torr 3: 85 percent / K2CO3 / acetone / 7 h / Heating 4: 80 percent / OsO4, N-methylmorpholine-N-oxide / H2O; acetone / 15 h 5: pyridine / 24 h / Ambient temperature 6: 0.50 g / NaOCH3 / methanol / 0.5 h / 50 - 60 °C View Scheme
参考文献
Synthetic Communications, , vol. 20, # 22 p. 3489 - 3496
反应条件
1: 50 percent / AlCl3 / various solvent(s) / 5 h / 70 °C 2: 90 percent / methanol / 24 h / Ambient temperature 3: 96 percent / H2 / 10percent Pd/C / ethanol / 4 h / 2327.2 Torr 4: 85 percent / K2CO3 / acetone / 7 h / Heating 5: 80 percent / OsO4, N-methylmorpholine-N-oxide / H2O; acetone / 15 h 6: pyridine / 24 h / Ambient temperature 7: 0.50 g / NaOCH3 / methanol / 0.5 h / 50 - 60 °C View Scheme
参考文献
Synthetic Communications, , vol. 20, # 22 p. 3489 - 3496
反应条件
1: 85 percent / K2CO3 / acetone / 7 h / Heating 2: 80 percent / OsO4, N-methylmorpholine-N-oxide / H2O; acetone / 15 h 3: pyridine / 24 h / Ambient temperature 4: 0.50 g / NaOCH3 / methanol / 0.5 h / 50 - 60 °C View Scheme
参考文献
Synthetic Communications, , vol. 20, # 22 p. 3489 - 3496
反应条件
1: 80 percent / OsO4, N-methylmorpholine-N-oxide / H2O; acetone / 15 h 2: pyridine / 24 h / Ambient temperature 3: 0.50 g / NaOCH3 / methanol / 0.5 h / 50 - 60 °C View Scheme
参考文献
Synthetic Communications, , vol. 20, # 22 p. 3489 - 3496
