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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5672-90-2
合成路线
（共 13 条）
5672-90-2
+
108-88-3
甲苯
→
反应条件
2142-03-2
+
2464-33-7
+
2314-76-3
2-(3-甲基苯基)-1H-异吲哚-1,3(2H)-二酮
反应条件
[iridium(III)(2-phenylpyridine)3] in acetonitrile T=20°C; 24 h; Sealed tubeIrradiation; Overall yield = 80percent; regioselective reaction;
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
110-86-1
吡啶
+
5672-90-2
→
反应条件
59208-49-0
+
19171-27-8
反应条件
[iridium(III)(2-phenylpyridine)3] in acetonitrile T=20°C; 24 h; Sealed tubeIrradiation; Overall yield = 41percent; Overall yield = 23 mg; regioselective reaction;
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
5672-90-2
+
71-43-2
苯
→
反应条件
520-03-6
N-苯基邻苯二甲酰亚胺
反应条件
[iridium(III)(2-phenylpyridine)3] in acetonitrile T=20°C; 24 h; Sealed tubeIrradiation; ConcentrationTime;
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
5672-90-2
+
98-08-8
三氟甲苯
→
反应条件
1555-31-3
+
314-11-4
+
314-81-8
反应条件
[iridium(III)(2-phenylpyridine)3] in acetonitrile T=20°C; 24 h; Sealed tubeIrradiation; Overall yield = 23percent; regioselective reaction;
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
110-00-9
呋喃
+
5672-90-2
→
反应条件
30739-23-2
反应条件
[iridium(III)(2-phenylpyridine)3] in acetonitrile T=20°C; 24 h; Sealed tubeIrradiation;
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
108-89-4
4-甲基吡啶
+
5672-90-2
→
反应条件
反应条件
[iridium(III)(2-phenylpyridine)3] in acetonitrile T=20°C; 24 h; Sealed tubeIrradiation; Overall yield = 57percent; Overall yield = 34 mg; regioselective reaction;
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
5672-90-2
+
108-88-3
甲苯
→
反应条件
2142-03-2
+
2464-33-7
+
2314-76-3
2-(3-甲基苯基)-1H-异吲哚-1,3(2H)-二酮
反应条件
[iridium(III)(2-phenylpyridine)3] in acetonitrile T=20°C; 24 h; Sealed tubeIrradiation; Overall yield = 80percent; regioselective reaction;
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
5672-90-2
+
100-66-3
苯甲醚
→
反应条件
2142-05-4
+
2314-77-4
+
2142-04-3
2-(4-甲氧基苯基)异吲哚-1,3-二酮
反应条件
[iridium(III)(2-phenylpyridine)3] in acetonitrile T=20°C; 24 h; Sealed tubeIrradiation; Overall yield = 81percent; regioselective reaction;
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
5672-90-2
+
108-88-3
甲苯
→
反应条件
2142-03-2
+
2464-33-7
+
2314-76-3
2-(3-甲基苯基)-1H-异吲哚-1,3(2H)-二酮
反应条件
[iridium(III)(2-phenylpyridine)3] in acetonitrile T=20°C; 24 h; Sealed tubeIrradiation; Overall yield = 80percent; regioselective reaction;
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
108-89-4
4-甲基吡啶
+
5672-90-2
→
反应条件
反应条件
[iridium(III)(2-phenylpyridine)3] in acetonitrile T=20°C; 24 h; Sealed tubeIrradiation; Overall yield = 57percent; Overall yield = 34 mg; regioselective reaction;
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
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