反应条件
1: sodium azide / H2O; acetone / 0 °C
2: CHCl3 / 50 °C
3: 70 percent / conc. hydrochloric acid / CHCl3
4: conc. hydrochloric acid, sodium nitrite / H2O / -6 °C
5: 70 percent / LiAlH4 / tetrahydrofuran / 24 h / Heating
View Scheme
参考文献
Miquel, Christian; Pigache, Pierre; Rigo, Benoit; Kolocouris, Nicolas
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 1447 - 1453
