9,10-二氢-9,10-乙桥蒽合成路线 (共 2 条)
反应条件
1: 75.3 percent / 95percent nitric acid/acetic anhydride / nitromethane / 24 h / 0 °C 2: 70.5 percent / 650 °C / 0.01 Torr View Scheme
参考文献
Baldwin, Jack E.; Swanson, Alistair G.; Cha, Jin Kun; Murphy, John A.
Tetrahedron, 1986 , vol. 42, # 14 p. 3943 - 3956
反应条件
1: 75.3 percent / 95percent nitric acid/acetic anhydride / nitromethane / 24 h / 0 °C
2: 99 percent / hydrazine hydrate, 10percent palladium on charcoal / ethanol / 2 h / Heating
3: 99 percent / pyridine / CHCl3 / 3.5 h / Ambient temperature
4: 86.5 percent / 650 °C / 0 Torr
View Scheme
参考文献
Baldwin, Jack E.; Swanson, Alistair G.; Cha, Jin Kun; Murphy, John A.
Tetrahedron, 1986 , vol. 42, # 14 p. 3943 - 3956