3-异丙氧基-3-氧代-丙酸合成路线 (共 7 条)
反应条件
piperidine in toluene Knoevenagel condensation; 35 h;
参考文献
Wang, Huan; Wei, Qing-Yi; Jiang, Hong; Jiang, Zhen-Hua
Research on Chemical Intermediates, 2012 , vol. 38, # 1 p. 207 - 213
反应条件
piperidine in toluene Knoevenagel condensation; 30 h;
参考文献
Wang, Huan; Wei, Qing-Yi; Jiang, Hong; Jiang, Zhen-Hua
Research on Chemical Intermediates, 2012 , vol. 38, # 1 p. 207 - 213
反应条件
in acetonitrile
22 h; Heating;
参考文献
Bulman Page, Philip C; Moore, Jonathan P.G; Mansfield, Ian; McKenzie, Michael J; Bowler, Wayne B; Gallagher, James A
Tetrahedron, 2001 , vol. 57, # 9 p. 1837 - 1847
反应条件
potassium hydroxide in tert-butyl alcohol
参考文献
Prosyanik, A.V.; Moskalenko, A.S.; Moretti, J.; Forni, A.; Torre, G.; Kostyanovskii, R.G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 4 p. 431 - 437
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 4 p. 525 - 532
反应条件
in isopropyl alcohol; toluene
T=85 - 90°C;
参考文献
Brock, Sally; Hose, David R.J.; Moseley, Jonathan D.; Parker, Alexandra J.; Patel, Ian; Williams, Andrew J.
Organic Process Research and Development, 2008 , vol. 12, # 3 p. 496 - 502
反应条件
boric acid
18 h; Reflux;
参考文献
Wang, Huan; Wei, Qing-Yi; Jiang, Hong; Jiang, Zhen-Hua
Research on Chemical Intermediates, 2012 , vol. 38, # 1 p. 207 - 213
反应条件
in diethyl ether
15 h; Ambient temperature; Yield given;
参考文献
Prosyanik, A.V.; Moskalenko, A.S.; Moretti, J.; Forni, A.; Torre, G.; Kostyanovskii, R.G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 4 p. 431 - 437
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 4 p. 525 - 532