3,3',4,4',5,5'-己甲氧基联苯合成路线 （共 21 条）
反应条件
palladium diacetate; potassium carbonate in water
T=25°C; 48 h;
参考文献
Santos-Filho, Everaldo F.; Sousa, Jokderlea C.; Bezerra, Natercia M.M.; Menezes, Paulo H.; Oliveira, Roberta A.
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5288 - 5291
反应条件
Wilkinson's catalyst; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical in 1,4-dioxane; water
T=130°C; 2 h; Inert atmosphere;
参考文献
Vogler, Thomas; Studer, Armido
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 13 p. 1963 - 1967
反应条件
zirconia-supported palladium; potassium carbonate in N,N-dimethyl-formamide
T=140°C; Ullmann type coupling; 5 h;
参考文献
Dumbre, Deepa K.; Wakharkar, Radhika D.; Choudhary, Vasant R.
Synthetic Communications, 2011 , vol. 41, # 2 p. 164 - 169
反应条件
sodium acetate; magnesium; palladium on activated charcoal in methanol
T=20°C; 24 h;
参考文献
Sajiki, Hironao; Mori, Akinori; Mizusaki, Tomoteru; Ikawa, Takashi; Maegawa, Tomohiro; Hirota, Kosaku
Organic Letters, 2006 , vol. 8, # 5 p. 987 - 990
反应条件
1: aq. K3PO4 / toluene / 0.5 h
2: Mg; methanol; NaOAc / Pd/C / 24 h / 20 °C
View Scheme
参考文献
Mori, Akinori; Mizusaki, Tomoteru; Ikawa, Takashi; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Chemistry - A European Journal, 2007 , vol. 13, # 5 p. 1432 - 1441
反应条件
1: With magnesium in tetrahydrofuran
T=20°C; 3 h; Inert atmosphere;
2: With synthetic air; cobalt(II) chloride in tetrahydrofuran
T=0°C; 0.5 h; Inert atmosphere;
参考文献
Mayer, Matthias; Czaplik, Waldemar Maximilian; Jacobi Von Wangelin, Axel
Synlett, 2009 , # 18 p. 2919 - 2923
反应条件
pyridine in chloroform
T=60°C;
参考文献
Combes; Finet; Siri
Journal of the Chemical Society. Perkin Transactions 1, 2002 , vol. 2, # 1 p. 38 - 44
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethylene glycol dimethyl ether
Suzuki cross-coupling; Heating;
参考文献
Gaukroger, Keira; Hadfield, John A.; Hepworth, Lucy A.; Lawrence, Nicholas J.; McGown, Alan T.
Journal of Organic Chemistry, 2001 , vol. 66, # 24 p. 8135 - 8138
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium chloride; sodium carbonate in ethanol; water; toluene
T=100°C; Suzuki-Miyaura coupling; 3 h; Inert atmosphere;
参考文献
Beaumard, Floriane; Dauban, Philippe; Dodd, Robert H.
Organic Letters, 2009 , vol. 11, # 8 p. 1801 - 1804
反应条件
1: H2 / Pd-C / ethanol
2: (i) NaNO2, aq. H2SO4, (ii) aq. KI
3: Cu, PhI / 240 °C
View Scheme
参考文献
Erdtman,H. et al.
Acta Chemica Scandinavica (1947-1973), 1963 , vol. 17, p. 1151 - 1156
