1-iodoundecane in N-dodecane Kinetics; React. performed at 50°C in mixt. of dodecane and naphtalene under Ar.; Ratio of 1-hexene: methylcyclopentane >20:1;

1-iodoundecane in N-dodecane Kinetics; React. performed at 50°C in mixt. of dodecane and naphtalene under Ar.; Ratio of 1-hexene: methylcyclopentane >20:1;

2,2'-azo-bisisobutyronitrile in benzene Refluxing in benzene (8 h, N2) after addn. of AIBN as a free radical initiator, quenching of react. mixt. by cooling in ice bath, low reactivity observed.; GLC anal. with n-dodecane as an added integration std.;

in diethyl ether refluxing with LiAlH4 for 3 h under N2;;

in toluene not isolated, detd. by GC/MS;

tetrachloromethane; 2,2'-azo-bisisobutyronitrile in tetrachloromethane byproducts: CHCl3; a soln. of Sn-compound in CCl4 was heated at 90°C for 2 h in thepresence of AIBN; evapd., recrystd. from C6H6; elem. anal.;