5-苄基-N-Cbz-L-谷氨酸酯合成路线 (共 13 条)
反应条件
sodium hydrogencarbonate 18 h; Ambient temperature;
参考文献
Desjardins, Michel; Garneau, Sylvie; Desgagnes, Julie; Lacoste, Lucille; Yang, Fu; Lapointe, Jacques; Chenevert, Robert
Bioorganic Chemistry, 1998 , vol. 26, # 1 p. 1 - 13
反应条件
1: aqueous HI 2: aqueous KHCO3 View Scheme
参考文献
Journal of the Chemical Society, , p. 3239,3243
反应条件
benzyl alcohol T=100°C;
参考文献
Chemische Berichte, , vol. 66, p. 1288,1290
反应条件
1: aqueous HI 2: aqueous KHCO3 View Scheme
参考文献
Journal of the Chemical Society, , p. 3239,3243
参考文献
Chemische Berichte, , vol. 95, p. 7 - 16
Chemische Berichte, , vol. 96, p. 204 - 212
反应条件
phosphorus pentachloride
参考文献
Hanby et al.
Journal of the Chemical Society, 1950 , p. 3239,3243
反应条件
1: 93 percent / DCC 2: 90 percent / H2 / Pd black / aq. acetic acid; methanol / 5 h View Scheme
参考文献
Lieflaender,M.
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1960 , vol. 320, p. 35 - 57
反应条件
1: tributylamine; chlorocarbonic acid ethyl ester; dioxane / anschliessendes Behandeln mit L-Alanin-benzylester-hydrochlorid und Tributylamin in Dioxan 2: Hydrogenation View Scheme
参考文献
Sachs; Brand
Journal of the American Chemical Society, 1953 , vol. 75, p. 4608
反应条件
hydrogen in ethanol 1.33333 h;
参考文献
Hemantha, Hosahalli P.; Sureshbabu, Vommina V.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 8 p. 2597 - 2601
反应条件
1: chlorocarbonic acid isobutyl ester; triethylamine; toluene / anschliessend Behandeln mit L-Tyrosin-benzylester-toluol-4-sulfonat in CHCl3 2: palladium; acetic acid; aqueous methanol / Hydrogenolyse View Scheme
参考文献
Lieflaender,M.
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1960 , vol. 320, p. 35 - 57