(S)-3-羟基丁酸乙酯合成路线 (共 42 条)
反应条件
hydrogenchloride; water 3 h;
参考文献
Hintzer, Klaus; Koppenhoefer, Bernhard; Schurig, Volker
Journal of Organic Chemistry, 1982 , vol. 47, # 20 p. 3850 - 3854
反应条件
hydrogen; palladium on activated charcoal in methanol Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 26, # 28 p. 3369 - 3372
反应条件
1: With dihydrogen peroxide in chloroform T=-20°C; 16 h; 2: With N-ethyl-N,N-diisopropylamine in chloroform T=30°C; 15 h; Further stages. Title compound not separated from byproducts.;
参考文献
Tetrahedron Letters, , vol. 48, # 34 p. 5976 - 5980
反应条件
Halobacterium halobium; pepton; potassium chloride; water; anhydrous trisodium citrate; magnesium sulfate; sodium chloride T=40°C; 120 h; Irradiation; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Helvetica Chimica Acta, , vol. 72, p. 793 - 799
反应条件
1: m-chloroperbenzoic acid / CH2Cl2 / -78 °C 2: aluminium amalgam View Scheme
参考文献
Tetrahedron Letters, , vol. 25, # 44 p. 5083 - 5086
反应条件
D-glucose in phosphate buffer T=30°C; pH=7; 12 h; Title compound not separated from byproducts.;
参考文献
Tetrahedron Asymmetry, , vol. 19, # 11 p. 1347 - 1351
反应条件
water; calcium carbonate
参考文献
Zheng, Jian-Feng; Lan, Hong-Qiao; Yang, Rui-Feng; Peng, Qi-Long; Xiao, Zhen-Hua; Tuo, Shi-Chuan; Hu, Kong-Zhen; Xiang, Yong-Gang; Wei, Zhen; Huang, Pei-Qiang; Zhang, Zhen
Helvetica Chimica Acta, 2012 , vol. 95, # 10 p. 1799 - 1808,10
反应条件
1: D-glucose / H2O; ethanol / Ambient temperature; baker's yeast; 30 min then 24 h 2: mCPBA 3: Al/Hg View Scheme
参考文献
Tetrahedron Letters, , vol. 27, # 44 p. 5405 - 5408
反应条件
1: triethylamine / dichloromethane 2: calcium carbonate; water View Scheme
参考文献
Helvetica Chimica Acta, , vol. 95, # 10 p. 1799 - 1808,10
反应条件
Candida antarctica lipase B T=23°C; Title compound not separated from byproducts.;
参考文献
Tetrahedron Asymmetry, , vol. 18, # 14 p. 1682 - 1687