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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
56821-03-5
合成路线
(共 7 条)
60344-80-1
→
反应条件
56821-03-5
反应条件
cupric(II) carbonate; sodium hydroxide; potassium carbonate in para-xylene Hydrolysis; 2 h; Heating;
参考文献
Eregowda; Kalpana; Hegde; Thimmaiah
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 4 p. 243 - 259
95-56-7
邻溴苯酚
→
反应条件
56821-03-5
反应条件
1: 70 percent / KOH / H2O / 5 h / 110 - 120 °C 2: 80 percent / Fe; glac. AcOH / H2O / Heating 3: 2 h / 140 - 160 °C 4: K2CO3; CuCO3 / p-xylene / 36 h / Heating 5: 75 percent / aq. NaOH; K2CO3; CuCO3 / p-xylene / 2 h / Heating View Scheme
参考文献
Eregowda; Kalpana; Hegde; Thimmaiah
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 4 p. 243 - 259
105837-78-3
→
反应条件
56821-03-5
反应条件
1: 80 percent / Fe; glac. AcOH / H2O / Heating 2: 2 h / 140 - 160 °C 3: K2CO3; CuCO3 / p-xylene / 36 h / Heating 4: 75 percent / aq. NaOH; K2CO3; CuCO3 / p-xylene / 2 h / Heating View Scheme
参考文献
Eregowda; Kalpana; Hegde; Thimmaiah
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 4 p. 243 - 259
105790-01-0
→
反应条件
56821-03-5
反应条件
1: 2 h / 140 - 160 °C 2: K2CO3; CuCO3 / p-xylene / 36 h / Heating 3: 75 percent / aq. NaOH; K2CO3; CuCO3 / p-xylene / 2 h / Heating View Scheme
参考文献
Eregowda; Kalpana; Hegde; Thimmaiah
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 4 p. 243 - 259
89-61-2
2,5-二氯硝基苯
→
反应条件
56821-03-5
反应条件
1: 70 percent / KOH / H2O / 5 h / 110 - 120 °C 2: 80 percent / Fe; glac. AcOH / H2O / Heating 3: 2 h / 140 - 160 °C 4: K2CO3; CuCO3 / p-xylene / 36 h / Heating 5: 75 percent / aq. NaOH; K2CO3; CuCO3 / p-xylene / 2 h / Heating View Scheme
参考文献
Eregowda; Kalpana; Hegde; Thimmaiah
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 4 p. 243 - 259
320785-96-4
→
反应条件
56821-03-5
反应条件
1: K2CO3; CuCO3 / p-xylene / 36 h / Heating 2: 75 percent / aq. NaOH; K2CO3; CuCO3 / p-xylene / 2 h / Heating View Scheme
参考文献
Eregowda; Kalpana; Hegde; Thimmaiah
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 4 p. 243 - 259
108953-08-8
→
反应条件
56821-03-5
反应条件
sulfuric acid; copper in ethanol Heating;
参考文献
Cieslak,J. et al.
Roczniki Chemii, 1960 , vol. 34, p. 103 - 110