3-(三甲基硅基)丙炔酸合成路线 （共 17 条）
反应条件
jones reagent in acetone T=0°C;
参考文献
Nicolaou, K. C.; Li, Wen Sen
Journal of the Chemical Society, Chemical Communications, 1985 , # 7 p. 421
反应条件
1: trimethylsilylacetylene With n-butyllithium in tetrahydrofuran; hexane T=78°C; 0.5 h; Inert atmosphere; 2: carbon dioxide in tetrahydrofuran; hexane T=20°C; 1 h;
参考文献
Lauber, Alex; Zelenay, Benjamin; Cvengros, Jan
Chemical Communications, 2014 , vol. 50, # 10 p. 1195 - 1197
参考文献
Laurence, Christian; Guilleme, Jean; Kirschleger, Bernard
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 1341 - 1343
参考文献
Cunico,R.F.; Lee,H.M.
Journal of the American Chemical Society, 1977 , vol. 99, p. 7613 - 7622
反应条件
quinoline; hydrogen; Lindlar's catalyst in hexane Ambient temperature;
参考文献
Hermeling, Dieter; Schaefer, Hans J.
Chemische Berichte, 1988 , vol. 121, p. 1151 - 1158
反应条件
quinoline; hydrogen; Lindlar's catalyst in methanol 7 h; Ambient temperature; Yield given;
参考文献
Fleming, Ian; Gil, Salvador; Sarkar, Achintya K.; Schmidlin, Tibur
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3351 - 3362
反应条件
Yield given. Multistep reaction;
参考文献
Hermeling, Dieter; Schaefer, Hans J.
Angewandte Chemie, 1984 , vol. 96, # 3 p. 238 - 239
Title/Abstract Full Text Show Details
Hermeling, Dieter; Schaefer, Hans J.
Chemische Berichte, 1988 , vol. 121, p. 1151 - 1158
反应条件
hydrogen; palladium on activated charcoal 1) 120 deg C, 18 h; 2) methanol; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Angewandte Chemie, , vol. 96, # 3 p. 238 - 239
反应条件
thionyl chloride beim anschliessenden Behandeln mit Aethanol;
参考文献
Monsanto Chem.Co.
Patent: US2887371 , 1954 ;
