5-溴-1,2,3,4,5-五苯基-1,3-环戊二烯合成路线 （共 6 条）
反应条件
hydrogen bromide; acetic acid RefluxInert atmosphere;
参考文献
Fischer, Daniel F.; Barakat, Assem; Xin, Zhuo-Qun; Weiss, Matthias E.; Peters, Rene
Chemistry - A European Journal, 2009 , vol. 15, # 35 p. 8722 - 8741
反应条件
1: 83 percent / aq. HCl / diethyl ether / 0.5 h / Heating 2: 81 percent / 48percent HBr / acetic acid; H2O / 0.17 h / Heating View Scheme
参考文献
Chemische Berichte, , vol. 121, p. 1745 - 1752
反应条件
1: 83 percent / aq. HCl / diethyl ether / 0.5 h / Heating 2: 81 percent / 48percent HBr / acetic acid; H2O / 0.17 h / Heating View Scheme
参考文献
Chemische Berichte, , vol. 121, p. 1745 - 1752
反应条件
hexacarbonylvanadium(0) 1.) n-hexane, 24 h, 30 deg C; 2.) water; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Priebsch, Wolfgang; Hoch, Martin; Rehder, Dieter
Chemische Berichte, 1988 , vol. 121, p. 1971 - 1976
反应条件
hydrogenchloride; n-butyllithium 1) THF, hexane, -78 deg C to -40 deg C, 2) THF, hexane;
参考文献
Janiak, Christoph; Schumann, Herbert; Stader, Carin; Wrackmeyer, Bernd; Zuckerman, Jerold J.
Chemische Berichte, 1988 , vol. 121, p. 1745 - 1752
反应条件
hexacarbonylvanadium(0) 1.) n-hexane, 24 h, 30 deg C; 2.) water; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Priebsch, Wolfgang; Hoch, Martin; Rehder, Dieter
Chemische Berichte, 1988 , vol. 121, p. 1971 - 1976
