3-甲基-2(3H)-噻唑硫酮合成路线 (共 7 条)
参考文献
Arbelot, M.; Allouche, A.; Purcell, K. F.; Chanon, M.
Journal of Organic Chemistry, 1995 , vol. 60, # 8 p. 2330 - 2343
反应条件
sodium tetrahydroborate in ethanol
T=0 - 20°C;
参考文献
Wolfe, Derek M.; Schreiner, Peter R.
European Journal of Organic Chemistry, 2007 , # 17 p. 2825 - 2838
反应条件
18-crown-6 ether in acetonitrile
0.5 h; Ambient temperature;
参考文献
Itoh, Takashi; Nagata, Kazuhiro; Okada, Mamiko; Ohsawa, Akio
Tetrahedron, 1993 , vol. 49, # 22 p. 4859 - 4870
反应条件
KO2 in dimethyl sulfoxide
0.5 h; Ambient temperature;
参考文献
Dondoni, Alessandro; Galliani, Guido; Mastellari, Annarosa; Medici, Alessandro
Tetrahedron Letters, 1985 , vol. 26, # 24 p. 2917 - 2920
参考文献
Huenig,S.; Sauer,G.
Justus Liebigs Annalen der Chemie, 1971 , vol. 748, p. 173 - 188
反应条件
sodium hydroxide
24 h; Ambient temperature;
参考文献
Kolosova,M.O.; Stavrovskaya,V.I.
J. Gen. Chem. USSR (Engl. Transl.), 1963 , vol. 33, p. 2778 - 2785,2706 - 2711
反应条件
1: With dibenzoyl peroxide in tetrahydrofuran
Heating;
2: With sodium bromide in diethyl ether; ethanol
Further stages.;
参考文献
Wolfe, Derek M.; Schreiner, Peter R.
European Journal of Organic Chemistry, 2007 , # 17 p. 2825 - 2838