2,8-二硝基-6,12-二苯基二苯并[b,f][1,5]二氮杂环辛四烯合成路线 (共 11 条)
反应条件
1: hydrazine hydrate / Raney nickel / aq. ethanol / 5 h / Heating 2: sodium acetate / acetic acid / 4 h / Heating View Scheme
参考文献
Kulkarni; Bishnoi; Dua
Journal of the Indian Chemical Society, 1990 , vol. 67, # 1 p. 48 - 51
反应条件
1: hydrazine hydrate / Raney nickel / aq. ethanol / 5 h / Heating 2: Et3N / benzene / 5 h / Heating View Scheme
参考文献
Kulkarni; Bishnoi; Dua
Journal of the Indian Chemical Society, 1990 , vol. 67, # 1 p. 48 - 51
反应条件
1: hydrazine hydrate / Raney nickel / aq. ethanol / 5 h / Heating 2: 2 h / Heating 3: 1) SOCl2 / 1) heating, 6 h, 2) reflux, 5 h View Scheme
参考文献
Kulkarni; Bishnoi; Dua
Journal of the Indian Chemical Society, 1990 , vol. 67, # 1 p. 48 - 51
反应条件
1: hydrazine hydrate / Raney nickel / aq. ethanol / 5 h / Heating 2: 2 h / Heating View Scheme
参考文献
Kulkarni; Bishnoi; Dua
Journal of the Indian Chemical Society, 1990 , vol. 67, # 1 p. 48 - 51
反应条件
1: hydrazine hydrate / Raney nickel / aq. ethanol / 5 h / Heating 2: CHCl3 / 24 h / Ambient temperature 3: K2CO3 / acetone / 6 h / Heating View Scheme
参考文献
Kulkarni; Bishnoi; Dua
Journal of the Indian Chemical Society, 1990 , vol. 67, # 1 p. 48 - 51
反应条件
1: hydrazine hydrate / Raney nickel / aq. ethanol / 5 h / Heating 2: 1.) conc. HCl, NaNO2 / 1.) <5 deg C, 2.) 1h, 80 deg C 3: K2CO3 / acetone / 6 h / Heating View Scheme
参考文献
Kulkarni; Bishnoi; Dua
Journal of the Indian Chemical Society, 1990 , vol. 67, # 1 p. 48 - 51
反应条件
1: hydrazine hydrate / Raney nickel / aq. ethanol / 5 h / Heating 2: CHCl3 / 24 h / Ambient temperature 3: Et3N / benzene / 6 h / Heating View Scheme
参考文献
Kulkarni; Bishnoi; Dua
Journal of the Indian Chemical Society, 1990 , vol. 67, # 1 p. 48 - 51
反应条件
1: hydrazine hydrate / Raney nickel / aq. ethanol / 5 h / Heating 2: 1.) conc. HCl, NaNO2 / 1.) <5 deg C, 2.) 1h, 80 deg C View Scheme
参考文献
Kulkarni; Bishnoi; Dua
Journal of the Indian Chemical Society, 1990 , vol. 67, # 1 p. 48 - 51
反应条件
1: hydrazine hydrate / Raney nickel / aq. ethanol / 5 h / Heating 2: sodium acetate / acetic acid / 4 h / Heating View Scheme
参考文献
Kulkarni; Bishnoi; Dua
Journal of the Indian Chemical Society, 1990 , vol. 67, # 1 p. 48 - 51
反应条件
1: hydrazine hydrate / Raney nickel / aq. ethanol / 5 h / Heating 2: ethanol / 8 h / Heating View Scheme
参考文献
Kulkarni; Bishnoi; Dua
Journal of the Indian Chemical Society, 1990 , vol. 67, # 1 p. 48 - 51