in pentane
introduction of B2H6 (from Na(BH4) and (C2H5)2O*BF3 in diglyme) in pentane soln.; evapn. of solvent and excess of substituted pyridine;; sublimation;;
参考文献
Weiner, M. A.; Lattman, M.
Inorganic and Nuclear Chemistry Letters, 1975 , vol. 11, p. 723 - 728
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Gmelin Handbook: B: B-Verb.14, 3.11.2, page 124 - 131