1-(2,2-二氟-1-苯基乙烯基)-4-氟苯合成路线 （共 35 条）
反应条件
copper(l) iodide; cesium fluoride in 1,4-dioxane; 1-methyl-pyrrolidin-2-one
T=20°C; 10 h; Glovebox; Reagent/catalystSolvent;
参考文献
Hu, Mingyou; He, Zhengbiao; Gao, Bing; Li, Lingchun; Ni, Chuanfa; Hu, Jinbo
Journal of the American Chemical Society, 2013 , vol. 135, # 46 p. 17302 - 17305
反应条件
sodium iodide in benzene
T=80°C; 36 h;
参考文献
Mloston, Grzegorz; Romanski, Jaroslaw; Heimgartner, Heinz
Heterocycles, 1999 , vol. 50, # 1 p. 403 - 410
反应条件
[Ni0(1,5-cyclooctadiene)2]; triphenylphosphine in tetrahydrofuran; diethyl ether
T=20°C; P=2625.26 Torr; 48 h; Product distribution / selectivity;
参考文献
Nagai, Takabumi; Shibanuma, Takashi; Ogoshi, Sensuke; Ohashi, Masato
Patent: US2012/330072 A1, 2012 ;
Location in patent: Page/Page column 7 ;
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=20°C; 4 h;
参考文献
Large-Radix, Sylvie; Billard, Thierry; Langlois, Bernard R.
Journal of Fluorine Chemistry, 2003 , vol. 124, # 2 p. 147 - 149
反应条件
triphenylphosphine; sodium iodide in tetrahydrofuran
T=70°C; 2 h;
参考文献
Nowak, Ireneusz; Robins, Morris J.
Organic Letters, 2005 , vol. 7, # 4 p. 721 - 724
反应条件
1: With copper(l) iodide; cesium fluoride in 1-methyl-pyrrolidin-2-one
T=20°C; 0.5 h; GloveboxSchlenk technique;
2: With water in 1-methyl-pyrrolidin-2-one
0.0833333 h; GloveboxSchlenk technique;
参考文献
Hu, Mingyou; He, Zhengbiao; Gao, Bing; Li, Lingchun; Ni, Chuanfa; Hu, Jinbo
Journal of the American Chemical Society, 2013 , vol. 135, # 46 p. 17302 - 17305
反应条件
in petroleum ether
20°C;
参考文献
Middleton,W.J. et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 1375 - 1384
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Gmelin Handbook: F: PerFHalOrg.1, 1.1.1.1, page 1 - 7
反应条件
P=0.05 Torr; Pyrolysis;
参考文献
Pohmakotr, Manat; Boonkitpattarakul, Kanhokthron; Ieawsuwan, Winai; Jarussophon, Suwatchai; Duangdee, Nongnaphat; Tuchinda, Patoomratana; Reutrakul, Vichai
Tetrahedron, 2006 , vol. 62, # 25 p. 5973 - 5985
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; cesium fluoride; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran; water
T=60°C; Suzuki-Miyaura Coupling; 6 h;
参考文献
Fujita, Takeshi; Suzuki, Naoto; Ichitsuka, Tomohiro; Ichikawa, Junji
Journal of Fluorine Chemistry, 2013 , vol. 155, p. 97 - 101
反应条件
in tetrahydrofuran
Heating;
参考文献
Obayashi, Michio; Ito, Eiji; Matsui, Kiyohide; Kondo, Kiyosi
Tetrahedron Letters, 1982 , vol. 23, # 22 p. 2323 - 2326
