反应条件
1: 8-mercapto-octanoic acid With n-butyllithium in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=0°C; 0.5 h; Inert atmosphere;
2: 1-bromo-octane in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=20°C; 20 h;
参考文献
Tremblay, Amy E.; Tan, Nigel; Whittle, Ed; Hodgson, Derek J.; Dawson, Brian; Buist, Peter H.; Shanklin, John
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 6 p. 1322 - 1328
