1-(2'-甲基[1,1'-联苯]-4-基)乙酮合成路线 (共 22 条)
反应条件
1: hydrogenchloride / water
2: triphenyl phosphite; K3PO4*3H2O; palladium diacetate; Ipr.HCl / tert-butyl alcohol / 6 h / 80 °C / |Inert atmosphere
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参考文献
Chen, Xiaofeng; Ke, Haihua; Chen, Yao; Guan, Changwei; Zou, Gang
Journal of Organic Chemistry, 2012 , vol. 77, # 17 p. 7572 - 7578
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium phosphate; n-butyllithium; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; potassium iodide
1.) dioxane, hexane, room temperature, 30 min, 2.) 70 deg C, 16 h; Yield given. Multistep reaction;
参考文献
Ueda, Masato; Saitoh, Atsushi; Oh-tani, Saori; Miyaura, Norio
Tetrahedron, 1998 , vol. 54, # 43 p. 13079 - 13086