6-甲氧基-2,3,4,5-四氢吡啶合成路线 （共 29 条）
反应条件
in anhydrous xylene; nitrogen; benzoic acid hydrazide; ethyl acetate
参考文献
Semiconductor Energy Laboratory Co., Ltd.
Patent: US2013/2131 A1, 2013 ;
反应条件
in xylene
1 h; Heating;
参考文献
Bonanomi, Michele; Baiocchi, Leandro
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1657 - 1660
反应条件
in diethyl ether
T=-24°C; 12 h;
参考文献
Zezza, Charles A.; Smith, Michael B.; Ross, Betsy A.; Arhin, Akwasi; Cronin, Patricia L. E.
Journal of Organic Chemistry, 1984 , vol. 49, # 23 p. 4397 - 4399
反应条件
1: 91 percent / methanol / 2 h / Ambient temperature
2: 90 percent / conc. aq. HCl
3: 86 percent / EtONa / ethanol / 1 h / Ambient temperature
View Scheme
参考文献
Dozorova, E. N.; Grizik, S. I.; Persianova, I. V.; Syubaev, R. D.; Shvarts, G. Ya.; Granik, V. G.
Pharmaceutical Chemistry Journal, 1985 , vol. 19, # 2 p. 100 - 104
Khimiko-Farmatsevticheskii Zhurnal, 1985 , vol. 19, # 2 p. 154 - 158
反应条件
1: 91 percent / methanol / 2 h / Ambient temperature
2: 81 percent / xylene / 7 h / Heating
View Scheme
参考文献
Dozorova, E. N.; Grizik, S. I.; Persianova, I. V.; Syubaev, R. D.; Shvarts, G. Ya.; Granik, V. G.
Pharmaceutical Chemistry Journal, 1985 , vol. 19, # 2 p. 100 - 104
Khimiko-Farmatsevticheskii Zhurnal, 1985 , vol. 19, # 2 p. 154 - 158
反应条件
1: 91 percent / methanol / 2 h / Ambient temperature
2: 81 percent / xylene / 7 h / Heating
3: 71 percent / alcoholic NH3 / 7 h / 150 °C
View Scheme
参考文献
Dozorova, E. N.; Grizik, S. I.; Persianova, I. V.; Syubaev, R. D.; Shvarts, G. Ya.; Granik, V. G.
Pharmaceutical Chemistry Journal, 1985 , vol. 19, # 2 p. 100 - 104
Khimiko-Farmatsevticheskii Zhurnal, 1985 , vol. 19, # 2 p. 154 - 158
反应条件
in diethyl ether
T=25°C; 12 h;
参考文献
Zezza, Charles A.; Smith, Michael B.; Ross, Betsy A.; Arhin, Akwasi; Cronin, Patricia L. E.
Journal of Organic Chemistry, 1984 , vol. 49, # 23 p. 4397 - 4399
反应条件
1: 41 percent / 14 h / 120 °C
2: 10 percent / H3BO3 / 1 h / 230 °C
View Scheme
参考文献
Delbecq, Philippe; Bacos, Daniel; Celerier, Jean Pierre; Lhommet, Gerard
Canadian Journal of Chemistry, 1991 , vol. 69, # 8 p. 1201 - 1206
反应条件
in N,N-dimethyl-formamide
1.5 h; Heating;
参考文献
Nilov; Granik
Russian Chemical Bulletin, 2006 , vol. 55, # 9 p. 1636 - 1641
