1: With 4,4,5,5-tetramethyl-[1,3,2]dioxaborolane; (.eta.(5)-indenyl)Ir(1,5-cyclooctadiene); 1,2-bis(dimethylphosphine)ethane T=150°C; 3.5 h; Inert atmosphere; 2: With Oxonereg;; water in acetone Cooling with ice;
参考文献
SOLVAY PHARMACEUTICALS B.V.
Patent: WO2009/115515 A1, 2009 ;
Location in patent: Page/Page column 44-45 ;
WO 2009/115515 A1
methanesulfonic acid; 1,3-dimethoxy benzene in toluene T=10°C;
参考文献
Davidson, James P.; Sarma, Keshab; Fishlock, Dan; Welch, Michael H.; Sukhtankar, Sunil; Lee, Gary M.; Martin, Michael; Cooper, Gary F.
Organic Process Research and Development, 2010 , vol. 14, # 2 p. 477 - 480
