反应条件
(2)H2O; methyllithium
1.) ether/TMEDA, -78 deg C, 30 min, 0 deg C, 3 h; 2.) -70 deg C, to room temperature; Yield given. Multistep reaction;
参考文献
Facchine, Kevin L.; Staley, Stuart W.; Zijl, Peter C. M. van; Mishra, Prasanna K.; Bothner-By, Aksel A.
Journal of the American Chemical Society, 1988 , vol. 110, # 15 p. 4900 - 4905
