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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
56982-37-7
合成路线
（共 21 条）
3058-39-7
4-碘氰基苯
+
3989-14-8
(4-甲氧基苯乙炔基)三甲基硅烷
→
反应条件
56982-37-7
反应条件
KOC(O)Ph; triphenylphosphine; copper(l) chloride in 1,3-dimethyl-imidazolidin-2-one T=120°C; Sila-Sonogashira-Hagihara cross-coupling reaction; 12 h; Inert atmosphere;
参考文献
Ihara, Hideki; Ueda, Akinori; Suginome, Michinori
Chemistry Letters, 2011 , vol. 40, # 9 p. 972 - 974
696-62-8
4-碘苯甲醚
+
75867-40-2
4-[(三甲基硅基)乙炔基]苄腈
→
反应条件
56982-37-7
反应条件
KOC(O)Ph; triphenylphosphine; copper(l) chloride in 1,3-dimethyl-imidazolidin-2-one T=120°C; Sila-Sonogashira-Hagihara cross-coupling reaction; 12 h; Inert atmosphere;
参考文献
Ihara, Hideki; Ueda, Akinori; Suginome, Michinori
Chemistry Letters, 2011 , vol. 40, # 9 p. 972 - 974
623-03-0
对氯苯甲腈
+
3989-14-8
(4-甲氧基苯乙炔基)三甲基硅烷
→
反应条件
56982-37-7
反应条件
(4R,5R)-DIOP; palladium diacetate; copper(l) chloride in N,N-dimethyl-formamide T=20 - 120°C; Sila-Sonogashira cross-coupling reaction;
参考文献
Nishihara, Yasushi; Inoue, Eiji; Noyori, Shintaro; Ogawa, Daisuke; Okada, Yoshiaki; Iwasaki, Masayuki; Takagi, Kentaro
Tetrahedron, 2012 , vol. 68, # 24 p. 4869 - 4881
696-62-8
4-碘苯甲醚
+
3058-39-7
4-碘氰基苯
+
14630-40-1
二(三甲基甲硅烷基)乙炔
→
反应条件
56982-37-7
反应条件
1: para-iodobenzonitrile; bis(trimethylsilyl)-acetylene With tetrakis(triphenylphosphine) palladium(0); copper(l) chloride in N,N-dimethyl-formamide T=80°C; sila-Sonogashira-Hagihara cross-coupling; 0.5 h; Inert atmosphere; 2: para-iodoanisole With tetrakis(triphenylphosphine) palladium(0); copper(l) chloride in N,N-dimethyl-formamide T=80°C; sila-Sonogashira-Hagihara cross-coupling; 9 h; Inert atmosphere;
参考文献
Nishihara, Yasushi; Inoue, Eiji; Noyori, Shintaro; Ogawa, Daisuke; Okada, Yoshiaki; Iwasaki, Masayuki; Takagi, Kentaro
Tetrahedron, 2012 , vol. 68, # 24 p. 4869 - 4881
104-92-7
4-溴苯甲醚
→
反应条件
56982-37-7
反应条件
tetrakis(triphenylphosphine) palladium(0); 1,8-diazabicyclo[5.4.0]undec-7-ene in dimethyl sulfoxide T=35 - 60°C; Sonogashira Cross-Coupling; 36 h;
参考文献
Park, Kyungho; Kim, Wonyoung; Lee, Sunwoo
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 10 p. 2859 - 2860
127591-24-6
+
3032-92-6
4-乙炔基苯甲腈
→
反应条件
56982-37-7
反应条件
oxygen; palladium diacetate in tetrahydrofuran T=25°C; Sonogashira coupling; P=760.051 Torr; 1.5 h;
参考文献
Pankajakshan, Sreekumar; Loh, Teck-Peng
Chemistry - An Asian Journal, 2011 , vol. 6, # 9 p. 2291 - 2295
3058-39-7
4-碘氰基苯
+
768-60-5
4-乙炔基苯甲醚
→
反应条件
56982-37-7
反应条件
pyrrolidine in water T=100°C; Sonogashira coupling; 7 h;
参考文献
Bernini, Roberta; Cacchi, Sandro; Fabrizi, Giancarlo; Forte, Giovanni; Petrucci, Francesco; Prastaro, Alessandro; Niembro, Sandra; Shafir, Alexandr; Vallribera, Adelina
Green Chemistry, 2010 , vol. 12, # 1 p. 150 - 158
→
反应条件
56982-37-7
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine in water; N,N-dimethyl-formamide T=120°C; 0.25 h; Microwave irradiation;
参考文献
Hou, Duen-Ren; Kuan, Ting-Chun; Li, Yu-Kai; Lee, Richmond; Huang, Kuo-Wei
Tetrahedron, 2010 , vol. 66, # 48 p. 9415 - 9420
696-62-8
4-碘苯甲醚
+
3032-92-6
4-乙炔基苯甲腈
→
反应条件
56982-37-7
反应条件
pyrrolidine in water T=100°C; Sonogashira coupling; 24 h;
参考文献
Bernini, Roberta; Cacchi, Sandro; Fabrizi, Giancarlo; Forte, Giovanni; Petrucci, Francesco; Prastaro, Alessandro; Niembro, Sandra; Shafir, Alexandr; Vallribera, Adelina
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 11 p. 2270 - 2273
104-92-7
4-溴苯甲醚
+
75867-40-2
4-[(三甲基硅基)乙炔基]苄腈
→
反应条件
56982-37-7
反应条件
copper(l) chloride; palladium dichloride; tris(p-fluoro phenyl)phosphine in N,N-dimethyl-formamide T=100°C; sila-Sonogashira-Hagihara cross-coupling; 12 h; Inert atmosphere;
参考文献
Nishihara, Yasushi; Inoue, Eiji; Noyori, Shintaro; Ogawa, Daisuke; Okada, Yoshiaki; Iwasaki, Masayuki; Takagi, Kentaro
Tetrahedron, 2012 , vol. 68, # 24 p. 4869 - 4881
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