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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
56983-95-0
合成路线
（共 38 条）
23031-08-5
+
588-72-7
→
反应条件
56983-95-0
反应条件
palladium bromide; tris(4-methoxyphenyl)-phosphine; silver benzoate in 1,4-dioxane T=125°C; 16 h; Inert atmosphere;
参考文献
Mousseau, James J.; Bull, James A.; Ladd, Carolyn L.; Fortier, Angelique; Sustac Roman, Daniela; Charette, Andre B.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8243 - 8261
13146-23-1
苯基乙酰基铜
+
23031-08-5
→
反应条件
56983-95-0
反应条件
1,4-diaza-bicyclo[2.2.2]octane; oxygen in chlorobenzene T=125°C; 24 h;
参考文献
Ding, Shengtao; Yan, Yuepeng; Jiao, Ning
Chemical Communications, 2013 , vol. 49, # 39 p. 4250 - 4252
1206884-59-4
→
反应条件
56983-95-0
反应条件
palladium bromide; tris(4-methoxyphenyl)-phosphine; silver benzoate in 1,4-dioxane T=125°C; 16 h; Inert atmosphere;
参考文献
Mousseau, James J.; Bull, James A.; Ladd, Carolyn L.; Fortier, Angelique; Sustac Roman, Daniela; Charette, Andre B.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8243 - 8261
51065-76-0
2-苯基吡唑并[1,5-a]吡啶-3-羧酸乙酯
→
反应条件
56983-95-0
反应条件
hydrogen bromide in water
参考文献
Zanka, Atsuhiko; Uematsu, Ryoichi; Morinaga, Yasuhiro; Yasuda, Hironobu; Yamazaki, Hiroshi
Organic Process Research and Development, 1999 , vol. 3, # 6 p. 389 - 393
23031-08-5
+
98-81-7
氢化松油醇
→
反应条件
56983-95-0
反应条件
palladium bromide; tris(4-methoxyphenyl)-phosphine; silver benzoate in 1,4-dioxane T=125°C; 16 h; Inert atmosphere;
参考文献
Mousseau, James J.; Bull, James A.; Ladd, Carolyn L.; Fortier, Angelique; Sustac Roman, Daniela; Charette, Andre B.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8243 - 8261
40949-56-2
1-[[(4-甲基苯基)磺酰基]氨基]-吡啶鎓氢氧化物内盐
+
536-74-3
苯乙炔
→
反应条件
56983-95-0
反应条件
potassium acetate; copper diacetate in 1,4-dioxane T=120°C; 16 h; Sealed tube;
参考文献
Ling, Lin; Chen, Jingqing; Song, Jiahui; Zhang, Yuhai; Li, Xinqian; Song, Lijuan; Shi, Feng; Li, Yuxue; Wu, Chunrui
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 23 p. 3894 - 3902
110-86-1
吡啶
→
反应条件
56983-95-0
反应条件
1.1: O-(2,4-dinitro-phenyl)-hydroxylamine / acetonitrile / 24 h / 40 °C / Inert atmosphere 2.1: sodium hydroxide / tetrahydrofuran; water / 0.08 h / 20 °C / Inert atmosphere 2.2: 5 h / Inert atmosphere 3.1: palladium bromide; tris(4-methoxyphenyl)-phosphine; silver benzoate / 1,4-dioxane / 16 h / 125 °C / Inert atmosphere View Scheme
参考文献
Mousseau, James J.; Bull, James A.; Ladd, Carolyn L.; Fortier, Angelique; Sustac Roman, Daniela; Charette, Andre B.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8243 - 8261
23031-08-5
→
反应条件
56983-95-0
反应条件
palladium bromide; tris(4-methoxyphenyl)-phosphine; silver benzoate in 1,4-dioxane T=125°C; 16 h; Inert atmosphere;
参考文献
Mousseau, James J.; Bull, James A.; Ladd, Carolyn L.; Fortier, Angelique; Sustac Roman, Daniela; Charette, Andre B.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8243 - 8261
23031-08-5
+
3240-11-7
苯乙炔-d
→
反应条件
56983-95-0
反应条件
palladium bromide; tris(4-methoxyphenyl)-phosphine; silver benzoate in 1,4-dioxane T=125°C; 16 h; Inert atmosphere;
参考文献
Mousseau, James J.; Bull, James A.; Ladd, Carolyn L.; Fortier, Angelique; Sustac Roman, Daniela; Charette, Andre B.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8243 - 8261
25275-41-6
→
反应条件
56983-95-0
反应条件
1.1: sodium hydroxide / tetrahydrofuran; water / 0.08 h / 20 °C / Inert atmosphere 1.2: 5 h / Inert atmosphere 2.1: palladium bromide; tris(4-methoxyphenyl)-phosphine; silver benzoate / 1,4-dioxane / 16 h / 125 °C / Inert atmosphere View Scheme
参考文献
Mousseau, James J.; Bull, James A.; Ladd, Carolyn L.; Fortier, Angelique; Sustac Roman, Daniela; Charette, Andre B.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8243 - 8261
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