反应条件
1.1: O-(2,4-dinitro-phenyl)-hydroxylamine / acetonitrile / 24 h / 40 °C / Inert atmosphere
2.1: sodium hydroxide / tetrahydrofuran; water / 0.08 h / 20 °C / Inert atmosphere
2.2: 5 h / Inert atmosphere
3.1: palladium bromide; tris(4-methoxyphenyl)-phosphine; silver benzoate / 1,4-dioxane / 16 h / 125 °C / Inert atmosphere
View Scheme
参考文献
Mousseau, James J.; Bull, James A.; Ladd, Carolyn L.; Fortier, Angelique; Sustac Roman, Daniela; Charette, Andre B.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8243 - 8261