反应条件
in further solvent(s)
other Radiation; Bi(NO3)3 dissolved in mannitol contained bromide, mixt. stirred, sonicated until dissolution, heated to 110 °C for 3 min (or 30 or 60 °C) kept at this temp. for 27 min (or 7, 17 min) in microwave reactor (irradiation power 500 W); mixt. cooled to room temp., centrifuged, washed (H2O, ethanol, 5 times),dried (dessicator, few d); detd. by XRD;
参考文献
Li, Guangfang; Qin, Fan; Yang, Hao; Lu, Zhong; Sun, Hongzhe; Chen, Rong
European Journal of Inorganic Chemistry, 2012 , # 15 p. 2508 - 2513
