1: oxalyl chloride / 3 h
2: 48 percent / dimethylformamide; diethyl ether / Ambient temperature
View Scheme
参考文献
Janusz, John M.; Buckwalter, Brian L.; Young, Patricia A.; LaHann, Thomas R.; Farmer, Ralph W.; et al.
Journal of Medicinal Chemistry, 1993 , vol. 36, # 18 p. 2595 - 2604
tert-butylhypochlorite; Ag(Phen)2OTf in acetonitrile
T=45°C; 25 h; Inert atmosphere;
参考文献
Wang, Zhentao; Zhu, Lin; Yin, Feng; Su, Zhongquan; Li, Zhaodong; Li, Chaozhong
Journal of the American Chemical Society, 2012 , vol. 134, # 9 p. 4258 - 4263