2-甲基-6-硝基苯胺合成路线 （共 113 条）
反应条件
1: 2-methyl-6-nitroazidobenzene With triphenylphosphine in diethyl ether T=20°C; 1 h; 2: isobutyraldehyde in chloroform aza-Wittig reaction; 144 h; Heating; 3: With carbon monoxide; 1,3-bis-(diphenylphosphino)propane; 1,10-phenanthroline monohydrate; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide T=70°C; P=4560.31 Torr; 21 h; Further stages.;
参考文献
Tetrahedron, , vol. 64, # 41 p. 9675 - 9684
反应条件
bromine; silver nitrate; triphenylphosphine in acetonitrile T=20°C; 0.0833333 h;
参考文献
Tetrahedron Letters, , vol. 47, # 38 p. 6879 - 6881
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 68, p. 88,89
反应条件
1: With nitric acid T=10 - 12°C; 2: With hydrogenchloride
参考文献
Liang, Yuxue; Gao, Shuang; Wan, Huihui; Wang, Junwei; Chen, Huilin; Zheng, Zhuo; Hu, Xinquan
Tetrahedron Asymmetry, 2003 , vol. 14, # 10 p. 1267 - 1273
参考文献
Takasago International Corporation
Patent: US5021593 A1, 1991 ;
反应条件
1: 60 percent / HNO3 2: concd. HCl / 7 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 114, # 25 p. 9869 - 9877
反应条件
(i) HNO3, (ii) aq. HCl; Multistep reaction;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 78, p. 571 - 582
反应条件
potassium tert-butylate; 1,1,1-trimethylhydrazinium iodide in dimethyl sulfoxide Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 61, # 9 p. 2934 - 2935
反应条件
nitric acid; acetic anhydride; acetic acid T=15 - 20°C; ueber mehrere Stufen;
参考文献
Chemische Berichte, , vol. 52, p. 1083
Chemische Berichte, , vol. 52, p. 1174
反应条件
ammonia T=150 - 160°C; unter Druck;
参考文献
Journal of the Chemical Society, , vol. 117, p. 856
