2-甲基-6-硝基苯胺合成路线 （共 113 条）
反应条件
1: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/, CuSO4, (iii) NO2/HNO3
2: aq. H2SO4
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参考文献
Haering,M.
Helvetica Chimica Acta, 1960 , vol. 43, p. 104 - 113
反应条件
1: 92 percent / N-chlorosuccinimide; AcOH
2: H2 / Raney-Ni / ethanol
3: aq. NaHCO3 / ethanol
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参考文献
Marterer, Wolfgang; Prikoszovich, Walter; Wiss, Jacques; Prashad, Mahavir
Organic Process Research and Development, 2003 , vol. 7, # 3 p. 318 - 323
反应条件
1: acetic acid; N-bromosuccinmide / 6 h / 50 - 55 °C / |Inert atmosphere
2: hydrogen / ethanol / 50 °C
3: sodium hydrogencarbonate / ethanol; water / 2.25 h / 25 °C / pH 6 - 8 / |Inert atmosphere
View Scheme
参考文献
Marterer, Wolfgang; Prikoszovich, Walter; Wiss, Jacques; Prashad, Mahavir
Organic Process Research and Development, 2003 , vol. 7, # 3 p. 318 - 323
