2-甲基-6-硝基苯胺合成路线 （共 113 条）
反应条件
1: glacial acetic acid / Diazotization 2: KOH-solution View Scheme
参考文献
Chemische Berichte, , vol. 37, p. 2583
反应条件
1: aq. HCl; SnCl2 2: 65 percent / thionyl chloride / benzene / 72 h View Scheme
参考文献
Vanelle, Patrice; Liegeois, Celine Tremblais; Meuche, Jacobine; Maldonado, Jose; Crozet, Michel P.
Heterocycles, 1997 , vol. 45, # 5 p. 955 - 962
反应条件
1: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/, CuSO4, (iii) NO2/HNO3 2: (i) aq. H2SO4, (ii) aq. NaNO2 View Scheme
参考文献
Helvetica Chimica Acta, , vol. 43, p. 104 - 113
反应条件
(i) HNO2, (ii) /BRN= 3587244/, (iii) H2SO4; Multistep reaction;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 78, p. 571 - 582
反应条件
1: 1.) aq. NaNO2, 2.) KI / 1.) 10 deg C, 30 min, 2.) H2O 2: 87 percent / Cu / dimethylformamide / 6 h / Heating 3: 1.) LiAlH4, 2.) air / 1.) ether, benzene, reflux, 4 h, 2.) ether, benzene 4: 47.5 percent / 800 °C / 0.6 Torr View Scheme
参考文献
Collman, James P.; Hutchison, James E.; Lopez, Michel Angel; Tabard, Alain; Guilard, Roger; Seok, Won K.; Ibers, James A.; L'Her, Maurice
Journal of the American Chemical Society, 1992 , vol. 114, # 25 p. 9869 - 9877
反应条件
1: 60 percent / N-bromosuccinimide / CCl4 2: 64 percent / NaNO2; AcOH 3: 85 percent / H2 / Pd/C / ethanol View Scheme
参考文献
Rakib; Benchidmi; Essassi; El Bouadili; Ibn Mansour; Bellan; Lopez; Lamande
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 5 p. 339 - 345
反应条件
1: 1.) aq. NaNO2, 2.) KI / 1.) 10 deg C, 30 min, 2.) H2O 2: 87 percent / Cu / dimethylformamide / 6 h / Heating 3: 1.) LiAlH4, 2.) air / 1.) ether, benzene, reflux, 4 h, 2.) ether, benzene 4: 47.5 percent / 800 °C / 0.6 Torr 5: 42.7 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 5 h / Heating View Scheme
参考文献
Collman, James P.; Hutchison, James E.; Lopez, Michel Angel; Tabard, Alain; Guilard, Roger; Seok, Won K.; Ibers, James A.; L'Her, Maurice
Journal of the American Chemical Society, 1992 , vol. 114, # 25 p. 9869 - 9877
反应条件
1: 80 percent / NaNO2; AcOH 2: 85 percent / Br2 / acetic acid / 5 h 3: 92 percent / H2 / Pd/C / ethanol View Scheme
参考文献
Rakib; Benchidmi; Essassi; El Bouadili; Ibn Mansour; Bellan; Lopez; Lamande
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 5 p. 339 - 345
反应条件
1: 80 percent / NaNO2; AcOH 2: 82 percent / Cl2 / acetic acid / 5 h View Scheme
参考文献
Rakib; Benchidmi; Essassi; El Bouadili; Ibn Mansour; Bellan; Lopez; Lamande
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 5 p. 339 - 345
反应条件
1: 80 percent / NaNO2; AcOH 2: Cl2 / acetic acid / 5 h 3: 91 percent / H2 / Pd/C / ethanol View Scheme
参考文献
Rakib; Benchidmi; Essassi; El Bouadili; Ibn Mansour; Bellan; Lopez; Lamande
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 5 p. 339 - 345
