N-(乙氧羰基)-L-缬氨酸合成路线 （共 4 条）
反应条件
1.1: SOCl2 / 0 - 20 °C 2.1: Mg 2.2: tetrahydrofuran / 0 - 20 °C 2.3: 53.35 g / sodium hydroxide / tetrahydrofuran / 3 h / 0 °C View Scheme
参考文献
Yu, Luo-Ting; Ho, Meng-Tsung; Chang, Ching-Yao; Yang, Teng-Kuei
Tetrahedron Asymmetry, 2007 , vol. 18, # 8 p. 949 - 962
反应条件
sodium hydroxide
2 h; Ambient temperaturepH=9-10;
参考文献
Ye, Tao; McKervey, M. Anthony
Tetrahedron, 1992 , vol. 48, # 37 p. 8007 - 8022
反应条件
sodium hydroxide; N-ethyl-N,N-diisopropylamine in water
1.) 0 deg C, 30 min; 2.) up to RT, 30 min;
参考文献
Chen, Francis M. F.; Benoiton, N. Leo
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1224 - 1227
反应条件
in water
T=0°C; 0.5 h;
参考文献
Noguchi, Takuya; Tehara, Naoka; Uesugi, Yuki; Jung, Seunghee; Imai, Nobuyuki
Chemistry Letters, 2012 , vol. 41, # 1 p. 42 - 43
