(3,4-二甲氧基苯基)乙醛合成路线 （共 41 条）
反应条件
dichloro bis(acetonitrile) palladium(II); water; oxygen; copper dichloride in toluene; tert-butyl alcohol T=60°C; Wacker Oxidation; P=6000.6 Torr; 1 h; Flow reactor;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 10 p. 1905 - 1910
反应条件
aq. acid 1 h; Ambient temperature;
参考文献
Stamos, Ioannis K.
Tetrahedron Letters, 1982 , vol. 23, # 4 p. 459 - 462
反应条件
1: p-toluenesulfonic acid / benzene / Heating 2: 99 percent / aq. acid / 1 h / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 23, # 4 p. 459 - 462
反应条件
1: 73 percent / NaOMe / methanol / -5 deg C, 2 h then 20 deg C, 3 h 2: 1) NaOMe/MeOH, 2) acetic acid / 1) benzene, H2O, Et2O, 5-10 deg C, 3 h, 2) benzene, reflux, 3h View Scheme
参考文献
Tetrahedron: Asymmetry, , vol. 1, # 1 p. 33 - 56
反应条件
1: in dichloromethane 0.25 h; 2: With silica gel in dichloromethane Further stages.;
参考文献
Tellitu, Imanol; Dominguez, Esther
Tetrahedron, 2008 , vol. 64, # 10 p. 2465 - 2470
反应条件
ruthenium trichloride; sodium periodate; N-benzyl-N,N,N-triethylammonium chloride in ethyl acetate T=20°C; 2 h; Title compound not separated from byproducts;
参考文献
Synthetic Communications, , vol. 33, # 22 p. 3947 - 3952
反应条件
diisobutylaluminium hydride in dichloromethane; cyclohexane T=0°C; 0.25 h;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 24 p. 6277 - 6282
Angew. Chem., , vol. 125, # 24 p. 6397 - 6402,6
反应条件
borane-THF; Dess-Martin periodane 1.) THF, 4 h, 2.) CH2Cl2, 1 h; Yield givenMultistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 64, # 2-5 p. 1720 - 1722
反应条件
1: 47 percent / copper chromite / quinoline / 0.5 h / 215 - 220 °C 2: 16 mg / 0.2 M HCl / dioxane; H2O / Heating View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 38, # 4 p. 323 - 326
反应条件
1: copper chromite / quinoline / Heating 2: 16 mg / 0.2 M HCl / dioxane; H2O / Heating View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 38, # 4 p. 323 - 326
