2-氨基异邻苯二甲酸二甲酯合成路线 （共 5 条）
反应条件
methanol in tetrahydrofuran; diethyl ether
T=20°C;
参考文献
ABBOTT LABORATORIES; WOODS, Keith W.; LAI, Chunqiu; PENNING, Thomas D.; MIYASHIRO, Julie
Patent: WO2013/12681 A1, 2013 ;
Location in patent: Page/Page column 80 ;
反应条件
palladium 10 on activated carbon; hydrogen in ethyl acetate
T=20°C; 20 h;
参考文献
Meiries, Sebastien; Le Duc, Gaetan; Chartoire, Anthony; Collado, Alba; Speck, Klaus; Arachchige, Kasun S. Athukorala; Slawin, Alexandra M. Z.; Nolan, Steven P.
Chemistry - A European Journal, 2013 , vol. 19, # 51 p. 17358 - 17368
反应条件
1: potassium permanganate; sodium hydroxide / water / 12 h / |Reflux
2: sulfuric acid / methanol / |Reflux
3: palladium 10 on activated carbon; hydrogen / ethyl acetate / 20 h / 20 °C
View Scheme
参考文献
Meiries, Sebastien; Le Duc, Gaetan; Chartoire, Anthony; Collado, Alba; Speck, Klaus; Arachchige, Kasun S. Athukorala; Slawin, Alexandra M. Z.; Nolan, Steven P.
Chemistry - A European Journal, 2013 , vol. 19, # 51 p. 17358 - 17368
反应条件
1: sulfuric acid / methanol / |Reflux
2: palladium 10 on activated carbon; hydrogen / ethyl acetate / 20 h / 20 °C
View Scheme
参考文献
Meiries, Sebastien; Le Duc, Gaetan; Chartoire, Anthony; Collado, Alba; Speck, Klaus; Arachchige, Kasun S. Athukorala; Slawin, Alexandra M. Z.; Nolan, Steven P.
Chemistry - A European Journal, 2013 , vol. 19, # 51 p. 17358 - 17368
反应条件
in acetic acid
2 h; Heating;
参考文献
Balli, Heinz; Zeller, Martin
Helvetica Chimica Acta, 1983 , vol. 66, # 7 p. 2135 - 2139
