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63148-62-9
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5706-08-1
合成路线
（共 6 条）
97677-81-1
2-(2-噻吩基)苯甲酰氯
→
反应条件
5706-08-1
反应条件
tin(IV) chloride in benzene T=0 - 10°C; Intramolecular Friedel-Crafts acylation; 0.5 h; Inert atmosphere;
参考文献
Pouchain, Laurent; Aleveque, Olivier; Nicolas, Yohann; Oger, Agathe; Regent, Charles-Henri Le; Allain, Magali; Blanchard, Philippe; Roncali, Jean
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1054 - 1064
7260-71-1
→
反应条件
5706-08-1
反应条件
1: N-bromosuccinmide / tetrachloromethane / 2.5 h / Reflux; Irradiation 2: water; silver nitrate / acetone / 0.17 h 3: Inert atmosphere; UV-irradiation View Scheme
参考文献
Bancerz, Mathew; Huck, Lawrence A.; Leigh, William J.; Mladenova, Gabriela; Najafian, Katayoun; Zeng, Xiaofeng; Lee-Ruff, Edward
Journal of Physical Organic Chemistry, 2010 , vol. 23, # 12 p. 1202 - 1213
773872-97-2
(2-噻吩-2-苯基)甲醇
→
反应条件
5706-08-1
反应条件
1: polyphosphoric acid / dichloromethane / 0.07 h / 120 °C 2: N-bromosuccinmide / tetrachloromethane / 2.5 h / Reflux; Irradiation 3: water; silver nitrate / acetone / 0.17 h 4: Inert atmosphere; UV-irradiation View Scheme
参考文献
Bancerz, Mathew; Huck, Lawrence A.; Leigh, William J.; Mladenova, Gabriela; Najafian, Katayoun; Zeng, Xiaofeng; Lee-Ruff, Edward
Journal of Physical Organic Chemistry, 2010 , vol. 23, # 12 p. 1202 - 1213
17595-84-5
→
反应条件
5706-08-1
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 0.67 h / 20 °C 2: polyphosphoric acid / dichloromethane / 0.07 h / 120 °C 3: N-bromosuccinmide / tetrachloromethane / 2.5 h / Reflux; Irradiation 4: water; silver nitrate / acetone / 0.17 h 5: Inert atmosphere; UV-irradiation View Scheme
参考文献
Bancerz, Mathew; Huck, Lawrence A.; Leigh, William J.; Mladenova, Gabriela; Najafian, Katayoun; Zeng, Xiaofeng; Lee-Ruff, Edward
Journal of Physical Organic Chemistry, 2010 , vol. 23, # 12 p. 1202 - 1213
610-97-9
2-碘苯甲酸甲酯
→
反应条件
5706-08-1
反应条件
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethanol; benzene / Inert atmosphere; Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 0.67 h / 20 °C 3: polyphosphoric acid / dichloromethane / 0.07 h / 120 °C 4: N-bromosuccinmide / tetrachloromethane / 2.5 h / Reflux; Irradiation 5: water; silver nitrate / acetone / 0.17 h 6: Inert atmosphere; UV-irradiation View Scheme
参考文献
Bancerz, Mathew; Huck, Lawrence A.; Leigh, William J.; Mladenova, Gabriela; Najafian, Katayoun; Zeng, Xiaofeng; Lee-Ruff, Edward
Journal of Physical Organic Chemistry, 2010 , vol. 23, # 12 p. 1202 - 1213
67-56-1
甲醇
+
1262850-01-0
→
反应条件
5706-08-1
+
7260-71-1
+
1262850-04-3
反应条件
Inert atmosphereUV-irradiation;
参考文献
Bancerz, Mathew; Huck, Lawrence A.; Leigh, William J.; Mladenova, Gabriela; Najafian, Katayoun; Zeng, Xiaofeng; Lee-Ruff, Edward
Journal of Physical Organic Chemistry, 2010 , vol. 23, # 12 p. 1202 - 1213
