4-(4-乙氧基苯基)-7-(4-甲氧基苯基)-2-甲基-5-氧代-4,6,7,8-四氢-1H-喹啉-3-羧酸丙酯合成路线 （共 13 条）
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane; water 24 h; Ambient temperature;
参考文献
Wang, Wuyi; Li, Tiechao; Attardo, Giorgio
Journal of Organic Chemistry, 1997 , vol. 62, # 19 p. 6598 - 6602
反应条件
1: zinc chloride; tetrachloromethane / Erhitzen des Reaktionsprodukts mit Kaliumcyanid in wss. Aethanol 2: aqueous sulfuric acid View Scheme
参考文献
Scientific Papers of the Institute of Physical and Chemical Research (Japan), , vol. 30, p. 180,188
反应条件
1: zinc chloride; tetrachloromethane / Erhitzen des Reaktionsprodukts mit Kaliumcyanid in wss. Aethanol 2: concentrated aqueous hydrochloric acid / 110 °C View Scheme
参考文献
Murahashi
Scientific Papers of the Institute of Physical and Chemical Research (Japan), 1936 , vol. 30, p. 180,188
反应条件
1: zinc chloride; tetrachloromethane / Erhitzen des Reaktionsprodukts mit Kaliumcyanid in wss. Aethanol 2: ethanolic KOH-solution 3: phosphorus oxychloride / Erwaermen des Reaktionsprodukts mit wss. Kalilauge View Scheme
参考文献
Murahashi
Scientific Papers of the Institute of Physical and Chemical Research (Japan), 1936 , vol. 30, p. 180,188
反应条件
argentic oxide
0.5 h; Ambient temperatureIrradiation;
参考文献
Ortiz; Walls; Yuste; Barrios; Sanchez-Obregon; Pinelo
Synthetic Communications, 1993 , vol. 23, # 6 p. 749 - 756
反应条件
ZSM-5 SiO2/Al2O3 50 in cyclohexane
T=120°C; 4 h; Product distribution / selectivity;
参考文献
DAVY PROCESS TECHNOLOGY LTD; COLLEY, Stephen William
Patent: WO2006/89900 A1, 2006 ;
Location in patent: Page/Page column 18 ;
反应条件
ZSM-5 SiO2/Al2O3 50 in cyclohexane
T=120°C; 4 h; Product distribution / selectivity;
参考文献
DAVY PROCESS TECHNOLOGY LTD; COLLEY, Stephen William
Patent: WO2006/89900 A1, 2006 ;
Location in patent: Page/Page column 15 ;
反应条件
sodium methylate
2 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
参考文献
Murahashi
Scientific Papers of the Institute of Physical and Chemical Research (Japan), 1936 , vol. 30, p. 180,188
反应条件
2 h; Ambient temperatureIrradiation; Yield given. Yields of byproduct given;
参考文献
Kirmse, Wolfgang; Kund, Klaus
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1465 - 1473
