3,4-二氨基二苯甲酮单盐酸盐合成路线 （共 6 条）
反应条件
hydrogen; nickel in tetrahydrofuran
参考文献
Dobrodei; El'tsov
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 620 - 629
反应条件
1: 1.) SOCl2, 2.) AlCl3 / 1.) reflux, 10 min, 2.) room temp., 24 h, then 40-50 deg C, 0.5 h 2: 80 percent / H2 / Raney nickel / tetrahydrofuran View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 68, # 4 p. 620 - 629
反应条件
1: 75 percent / CrO3, aq. H2SO4 / 1.) 35 deg C, 0.5 h, 2.) 45-55 deg C, 4 h 2: 1.) SOCl2, 2.) AlCl3 / 1.) reflux, 10 min, 2.) room temp., 24 h, then 40-50 deg C, 0.5 h 3: 80 percent / H2 / Raney nickel / tetrahydrofuran View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 68, # 4 p. 620 - 629
反应条件
1: 8 g / aq. HNO3 / 0.08 h 2: 75 percent / CrO3, aq. H2SO4 / 1.) 35 deg C, 0.5 h, 2.) 45-55 deg C, 4 h 3: 1.) SOCl2, 2.) AlCl3 / 1.) reflux, 10 min, 2.) room temp., 24 h, then 40-50 deg C, 0.5 h 4: 80 percent / H2 / Raney nickel / tetrahydrofuran View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 68, # 4 p. 620 - 629
反应条件
1: 89 percent / K2S2O8, H2SO4 / 24 h 2: 8 g / aq. HNO3 / 0.08 h 3: 75 percent / CrO3, aq. H2SO4 / 1.) 35 deg C, 0.5 h, 2.) 45-55 deg C, 4 h 4: 1.) SOCl2, 2.) AlCl3 / 1.) reflux, 10 min, 2.) room temp., 24 h, then 40-50 deg C, 0.5 h 5: 80 percent / H2 / Raney nickel / tetrahydrofuran View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 68, # 4 p. 620 - 629
反应条件
1: 6 g / sodium hydroxide / H2O / 12 h / Heating 2: 0.1 g / pyridine / Ambient temperature View Scheme
参考文献
Viswanathan, N.; Sidhaye, A. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 948 - 951
