2-氨基-6-硝基苯甲酸甲酯合成路线 （共 6 条）
反应条件
sodium hydrogencarbonate; triethylamine; sodium chloride in N,N-dimethyl-formamide
参考文献
Merck and Co., Inc.
Patent: US4847294 A1, 1989 ;
反应条件
triethylamine in N,N-dimethyl-formamide 18 h; Ambient temperature;
参考文献
Saari; Schwering
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 4 p. 1253 - 1255
反应条件
acetic acid 0.5 h; Heating;
参考文献
Rewcastle, Gordon W.; Denny, William A.
Synthesis, 1985 , # 2 p. 220 - 222
反应条件
1: SOCl2 / Heating 2: NaN3 / H2O; acetone / 0.25 h 3: 84 percent / aq. acetic acid / 0.5 h / Heating View Scheme
参考文献
Synthesis, , # 2 p. 220 - 222
反应条件
1: NaN3 / H2O; acetone / 0.25 h 2: 84 percent / aq. acetic acid / 0.5 h / Heating View Scheme
参考文献
Synthesis, , # 2 p. 220 - 222
反应条件
1: 1) Aq. sodium nitrite, aq. HCl, 2) cupric chloride, sulfur dioxide / 1) Acetic acid, -5 to 0 deg C, 30 min, 2) 0 deg C, 3 h, room temperature 18 h.
2: Conc. ammonium hydroxide / 18 h / Ambient temperature
View Scheme
参考文献
Saari; Schwering
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 4 p. 1253 - 1255
