螺[3.4]-6-辛烯-1,3-二酮合成路线 （共 3 条）
反应条件
hydrogenchloride in water
T=20°C; 24 h;
参考文献
Brand, Stephen; De Candole, Benjamin C.; Brown, Julien A.
Organic Letters, 2003 , vol. 5, # 13 p. 2343 - 2346
反应条件
1: oxalyl chloride; DMF / CH2Cl2 / 2 h / 20 °C
2: 73 percent / triethylamine / diethyl ether; hexane / 168 h / 45 °C
3: 65 percent / hydrochloric acid / H2O / 24 h / 20 °C
View Scheme
参考文献
Brand, Stephen; De Candole, Benjamin C.; Brown, Julien A.
Organic Letters, 2003 , vol. 5, # 13 p. 2343 - 2346
反应条件
1: 73 percent / triethylamine / diethyl ether; hexane / 168 h / 45 °C
2: 65 percent / hydrochloric acid / H2O / 24 h / 20 °C
View Scheme
参考文献
Brand, Stephen; De Candole, Benjamin C.; Brown, Julien A.
Organic Letters, 2003 , vol. 5, # 13 p. 2343 - 2346
