4'-(十二烷氧基)[1,1'-联苯]-4-甲腈合成路线 （共 4 条）
反应条件
potassium carbonate in acetone
35 h; Heating;
参考文献
Amako, Masaaki; Schinkel, Jonathan; Freiburger, Lee; Brook, Michael A.
Dalton Transactions, 2005 , # 1 p. 74 - 81
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; potassium phosphate in water; toluene
T=80°C; Suzuki-Miyaura cross-coupling; 8 h;
参考文献
Maly, Kenneth E.; Dauphin, Caroline; Wuest, James D.
Journal of Materials Chemistry, 2006 , vol. 16, # 48 p. 4695 - 4700
反应条件
1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate / isopropyl alcohol; water / 15 h / 70 °C / |Inert atmosphere
2: potassium carbonate; potassium iodide / acetone / 72 h / |Reflux
View Scheme
参考文献
Dutronc, Thibault; Terazzi, Emmanuel; Guenee, Laure; Buchwalder, Kerry-Lee; Spoerri, Aurore; Emery, Daniel; Mareda, Jiri; Floquet, Sebastien; Piguet, Claude
Chemistry - A European Journal, 2013 , vol. 19, # 26 p. 8447 - 8456
反应条件
1: hydrogenchloride; water / 0.5 h
2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate / isopropyl alcohol; water / 15 h / 70 °C / |Inert atmosphere
3: potassium carbonate; potassium iodide / acetone / 72 h / |Reflux
View Scheme
参考文献
Dutronc, Thibault; Terazzi, Emmanuel; Guenee, Laure; Buchwalder, Kerry-Lee; Spoerri, Aurore; Emery, Daniel; Mareda, Jiri; Floquet, Sebastien; Piguet, Claude
Chemistry - A European Journal, 2013 , vol. 19, # 26 p. 8447 - 8456
