water in tetrahydrofuran slow addn. of 10 mmol of the Grignard reagent to a stirred soln. of borane in THF (40 mmol); the mixt. was poured into ice-water and acidified with 10percent HCl;; extn. into ether three-times; the combined extracts were dried over NaSO4; removal of solvent under reduced pressure; trituration with petroleum ether; recrystn. from H2O;;
参考文献
Kabalka, George W.; Sastry, Usha; Sastry, K.A.R.; Knapp, Furn F.; Srivastava, Prem C.
Journal of Organometallic Chemistry, 1983 , vol. 259, # 3 p. 269 - 274
Qian, Yimin; Marugan, Juan Jose; Fossum, Renae D.; Vogt, Andreas; Sebti, Said M.; Hamilton, Andrew D.
Bioorganic and Medicinal Chemistry, 1999 , vol. 7, # 12 p. 3011 - 3024
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in diethyl ether 0.5 h; Heating;
参考文献
Pham, Chiem Van; Burkhardt, A.; Shabana, R.; Cunningham, David D.; Mark, Harry B.; Zimmer, Hans
Phosphorus, Sulfur and Silicon and the Related Elements, 1989 , vol. 46, p. 153 - 168
