Weinmayr
Journal of the American Chemical Society, 1952 , vol. 74, p. 4353,4356
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Goncalves et al.
Journal of Organic Chemistry, 1952 , vol. 17, p. 705,709
in diethyl ether; toluene
byproducts: MgBr2; toluene soln. of stannane added to organomagnesium compd. (prepd. in dry ether); heated at the b.p. of toluene (ether distd. off) until a test for bromine was neg. (3 h); cooled; hydrolyzed; org. layer sepd., washed, dried, solvent driven off; recrystd. (propyl alcohol); elem. anal.; IR; PMR;
参考文献
Lapkin, I. I.; Dumler, V. A.; Evstafeeva, N. E.; Kolbasina, V. D.; Konyukhova, L. M.
Journal of General Chemistry USSR (English Translation), 1983 , vol. 53, p. 1645 - 1647
Zhurnal Obshchei Khimii, 1983 , vol. 53, p. 1828 - 1831
in diethyl ether; toluene
byproducts: MgBr2; toluene soln. of stannane added to organomagnesium compd. (prepd. in dry ether); heated at the b.p. of toluene (ether distd. off) until a test for bromine was neg. (15 h); cooled; hydrolyzed; org. layer sepd., washed, dried, solvent driven off; recrystd. (propyl alcohol); IR; PMR; elem. anal.;
参考文献
Lapkin, I. I.; Dumler, V. A.; Evstafeeva, N. E.; Kolbasina, V. D.; Konyukhova, L. M.
Journal of General Chemistry USSR (English Translation), 1983 , vol. 53, p. 1645 - 1647
Zhurnal Obshchei Khimii, 1983 , vol. 53, p. 1828 - 1831
in diethyl ether; toluene
byproducts: MgBr2; toluene soln. of stannane added to organomagnesium compd. (prepd. in dry ether); heated at the b.p. of toluene (ether distd. off) until a test for bromine was neg. (4 h); cooled; hydrolyzed; org. layer sepd., washed, dried, solvent driven off; recrystd. (propyl alcohol); IR; PMR; elem. anal.;
参考文献
Lapkin, I. I.; Dumler, V. A.; Evstafeeva, N. E.; Kolbasina, V. D.; Konyukhova, L. M.
Journal of General Chemistry USSR (English Translation), 1983 , vol. 53, p. 1645 - 1647
Zhurnal Obshchei Khimii, 1983 , vol. 53, p. 1828 - 1831
