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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
57132-25-9
合成路线
（共 13 条）
16927-82-5
→
反应条件
57132-25-9
反应条件
1: With hydrogen; palladium in ethanol 2: With N-methyl-2-indolinone; tetrapropylammonium perruthennate in dichloromethane
参考文献
Nakamura, Mitsuhiro; Mamino, Masashi; Masaki, Mizuki; Maki, Shojiro; Matsui, Ryo; Kojima, Satoshi; Hirano, Takashi; Ohmiya, Yoshihiro; Niwa, Haruki
Tetrahedron Letters, 2005 , vol. 46, # 1 p. 53 - 56
598-32-3
3-丁烯-2-醇
+
18684-09-8
→
反应条件
57132-25-9
反应条件
tetrabutylammomium bromide; oxygen; palladium diacetate in dimethyl sulfoxide; N,N-dimethyl-formamide T=70°C; Heck Reaction; P=760.051 Torr; Schlenk technique;
参考文献
Huang, Liangbin; Qi, Ji; Wu, Xia; Wu, Wanqing; Jiang, Huanfeng
Chemistry - A European Journal, 2013 , vol. 19, # 46 p. 15462 - 15466
95-46-5
邻溴甲苯
+
78-94-4
丁烯酮
→
反应条件
57132-25-9
反应条件
tetrabutylammomium bromide; tetra-(n-butyl)ammonium iodide; niobium bromide in pyridine; N,N-dimethyl-formamide T=70°C; Electrochemical reaction;
参考文献
Condon, Sylvie; Dupre, Daniel; Falgayrac, Gilles; Nedelec, Jean-Yves
European Journal of Organic Chemistry, 2002 , # 1 p. 105 - 111
201230-82-2
+
16419-60-6
2-甲基苯硼酸
+
78-94-4
丁烯酮
→
反应条件
57132-25-9
+
195137-30-5
反应条件
RhH(CO)(triphenylphosphine)3 in methanol T=60°C; P=30002.4 Torr; 18 h;
参考文献
Sauthier, Mathieu; Castanet, Yves; Mortreux, Andre
Chemical Communications, 2004 , # 13 p. 1520 - 1521
95-46-5
邻溴甲苯
→
反应条件
57132-25-9
反应条件
1.1: 49 percent / PPh3; Et3N / Pd(OAc)2 / dimethylformamide 2.1: H2 / Pd black / ethanol 2.2: 82 percent / tetrapropylammonium perruthenate; NMO / CH2Cl2 View Scheme
参考文献
Nakamura, Mitsuhiro; Mamino, Masashi; Masaki, Mizuki; Maki, Shojiro; Matsui, Ryo; Kojima, Satoshi; Hirano, Takashi; Ohmiya, Yoshihiro; Niwa, Haruki
Tetrahedron Letters, 2005 , vol. 46, # 1 p. 53 - 56
104075-51-6
→
反应条件
57132-25-9
反应条件
sodium chloride in water; dimethyl sulfoxide T=160°C; 7 h; Yield given;
参考文献
Fehr, Charles; Galindo, Jose; Haubrichs, Rolf; Perret, Roland
Helvetica Chimica Acta, 1989 , vol. 72, p. 1537 - 1553
16927-82-5
→
反应条件
57132-25-9
反应条件
hydrogen; palladium in ethanol Title compound not separated from byproducts;
参考文献
Nakamura, Mitsuhiro; Mamino, Masashi; Masaki, Mizuki; Maki, Shojiro; Matsui, Ryo; Kojima, Satoshi; Hirano, Takashi; Ohmiya, Yoshihiro; Niwa, Haruki
Tetrahedron Letters, 2005 , vol. 46, # 1 p. 53 - 56
16927-82-5
→
反应条件
57132-25-9
+
57132-23-7
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; sodium formate; N-(2-amino-ethyl)-4-methyl-benzenesulphonamide in water T=60°C; 5 h; Inert atmosphere; chemoselective reaction;
参考文献
Li, Xuefeng; Li, Liangchun; Tang, Yuanfu; Zhong, Ling; Cun, Linfeng; Zhu, Jin; Liao, Jian; Deng, Jingen
Journal of Organic Chemistry, 2010 , vol. 75, # 9 p. 2981 - 2988
201230-82-2
+
78-94-4
丁烯酮
→
反应条件
57132-25-9
+
195137-30-5
反应条件
methanol; [RhCl(η2:η2-cycloocta-1,5-diene)]2; triphenylphosphine T=80°C; P=15001.5 Torr; 18 h; AutoclaveInert atmosphere;
参考文献
Sauthier, Mathieu; Lamotte, Nicolas; Dheur, Julien; Castanet, Yves; Mortreux, Andre
New Journal of Chemistry, 2009 , vol. 33, # 5 p. 969 - 971
552-45-4
邻甲基氯化苄
→
反应条件
57132-25-9
反应条件
1: 70 percent / K2CO3 / toluene / 20 h / 100 °C 2: NaCl / dimethylsulfoxide; H2O / 7 h / 160 °C View Scheme
参考文献
Fehr, Charles; Galindo, Jose; Haubrichs, Rolf; Perret, Roland
Helvetica Chimica Acta, 1989 , vol. 72, p. 1537 - 1553
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