3Beta-羟基-5-雄烯-17-酮 3-葡糖苷酸合成路线 （共 6 条）
反应条件
Escherichia coli glucuronylsynthase mutant E504G; n-dodecyl β-D-glucopyranosyl-(1-gt;4)-β-D-glucopyranoside
T=20°C; pH=7.5; 96 h; aq. phosphate buffer;
参考文献
Wilkinson, Shane M.; Watson, Morgan A.; Willis, Anthony C.; McLeod, Malcolm D.
Journal of Organic Chemistry, 2011 , vol. 76, # 7 p. 1992 - 2000
反应条件
1: silver carbonate; diethyl ether
2: methanol; barium hydroxide; water
View Scheme
参考文献
Pelzer
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1959 , vol. 314, p. 234,239
反应条件
1: silver carbonate; diethyl ether
2: methanol; barium hydroxide; water
View Scheme
参考文献
Pelzer
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1959 , vol. 314, p. 234,239
反应条件
methanol; barium dihydroxide; water
参考文献
Wotiz et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 1704,1706
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Schapiro
Biochemical Journal, 1939 , vol. 33, p. 385,387
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Pelzer
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1959 , vol. 314, p. 234,239
反应条件
1: sodium hypochlorite; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hydroxide / water / 3 h / 4 °C / pH 9.5
2: histidine-6 tagged glucuronylsynthase E504G mutant from Escherichia coli strain GMS407(DE3) / 21 °C / pH 7.5 / aq. phosphate buffer; Enzymatic reaction
View Scheme
参考文献
Wilkinson, Shane M.; Watson, Morgan A.; Willis, Anthony C.; McLeod, Malcolm D.
Journal of Organic Chemistry, 2011 , vol. 76, # 7 p. 1992 - 2000
反应条件
1: histidine-6 tagged glucuronylsynthase E504G mutant from Escherichia coli strain GMS407(DE3) / 21 °C / pH 7.5 / aq. phosphate buffer; Enzymatic reaction
2: titanium(III) chloride; ammonium acetate; water; acetic acid / 1,4-dioxane / 2 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Wilkinson, Shane M.; Watson, Morgan A.; Willis, Anthony C.; McLeod, Malcolm D.
Journal of Organic Chemistry, 2011 , vol. 76, # 7 p. 1992 - 2000
