2,2-二氯-1-(4-甲基苯基)-1-丙酮合成路线 (共 9 条)
反应条件
hydrogen; methylamine; palladium on barium sulfate in methanol
参考文献
Bratchanskii,P.E.; Komissarova,G.G.
Zhurnal Organicheskoi Khimii, 1975 , vol. 11, p. 1661 - 1665,1650 - 1654
反应条件
sulfuric acid in tetrahydrofuran
4 h; Ambient temperature;
参考文献
Barluenga, Jose; Tomas, Miguel; Lopez-Ortiz, J. Francisco; Gotor, Vicente
Synthesis, 1984 , # 11 p. 935 - 936
反应条件
1: N-chlorosuccinimide / toluene
2: aq. sulfuric acid / tetrahydrofuran / 4 h / Ambient temperature
View Scheme
参考文献
Barluenga, Jose; Tomas, Miguel; Lopez-Ortiz, J. Francisco; Gotor, Vicente
Synthesis, 1984 , # 11 p. 935 - 936
反应条件
1: N-chlorosuccinimide / toluene
2: aq. sulfuric acid / tetrahydrofuran / 4 h / Ambient temperature
View Scheme
参考文献
Barluenga, Jose; Tomas, Miguel; Lopez-Ortiz, J. Francisco; Gotor, Vicente
Synthesis, 1984 , # 11 p. 935 - 936
反应条件
1: 91 percent / N-chlorosuccinimide / toluene / 3 h / 50 °C
2: aq. sulfuric acid / tetrahydrofuran / 4 h / Ambient temperature
View Scheme
参考文献
Barluenga, Jose; Tomas, Miguel; Lopez-Ortiz, J. Francisco; Gotor, Vicente
Synthesis, 1984 , # 11 p. 935 - 936
反应条件
1: 86 percent / N-chlorosuccinimide / toluene / 3 h / 50 °C
2: aq. sulfuric acid / tetrahydrofuran / 4 h / Ambient temperature
View Scheme
参考文献
Barluenga, Jose; Tomas, Miguel; Lopez-Ortiz, J. Francisco; Gotor, Vicente
Synthesis, 1984 , # 11 p. 935 - 936
反应条件
1: 87 percent / N-chlorosuccinimide / toluene / 3 h / 50 °C
2: 86 percent / aq. sulfuric acid / tetrahydrofuran / 4 h / Ambient temperature
View Scheme
参考文献
Barluenga, Jose; Tomas, Miguel; Lopez-Ortiz, J. Francisco; Gotor, Vicente
Synthesis, 1984 , # 11 p. 935 - 936
反应条件
sulfuric acid in tetrahydrofuran
4 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Barluenga, Jose; Tomas, Miguel; Lopez-Ortiz, J. Francisco; Gotor, Vicente
Synthesis, 1984 , # 11 p. 935 - 936
反应条件
sulfuric acid in tetrahydrofuran
4 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Barluenga, Jose; Tomas, Miguel; Lopez-Ortiz, J. Francisco; Gotor, Vicente
Synthesis, 1984 , # 11 p. 935 - 936