3-羟基-5-甲氧基苯甲醛合成路线 （共 13 条）
反应条件
1: chloroform; phosphorus pentachloride
2: palladium-barium sulfate; toluene / 110 °C / Hydrogenation.und Verseifung des entstandenen 3-Methoxy-5-carbomethoxyoxy-benzaldehyds mit waessrig-alkoholischer Natronlauge in Wasserstoff-Atmosphaere
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参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1927 , vol. <2> 116, p. 323
反应条件
1: 84 percent / triethylamine / tetrahydrofuran
2: 74 percent / BH3*THF / tetrahydrofuran / 12 h
3: 80 percent / PBr3 / tetrahydrofuran / 2 h
4: 56 percent / 1-methyl-pyrrolidin-2-one / 5 h
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参考文献
Weist, Stefan; Kittel, Claudia; Bischoff, Daniel; Bister, Bojan; Pfeifer, Volker; Nicholson, Graeme J.; Wohlleben, Wolfgang; Suessmuth, Roderich D.
Journal of the American Chemical Society, 2004 , vol. 126, # 19 p. 5942 - 5943
反应条件
triethylamine in tetrahydrofuran
参考文献
Weist, Stefan; Kittel, Claudia; Bischoff, Daniel; Bister, Bojan; Pfeifer, Volker; Nicholson, Graeme J.; Wohlleben, Wolfgang; Suessmuth, Roderich D.
Journal of the American Chemical Society, 2004 , vol. 126, # 19 p. 5942 - 5943
