bis(acetylacetonate)nickel(II); SCl2; diisobutylaluminium hydride 1) hexane, 5 deg C, 20 h, 2) toluene, r.t., 2 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;

sodium hydroxide; sodium tetrahydroborate; SCl2 1) hexane, 5 deg C, 20 h, 2) DMFA, H2O, 50-55 deg C, 2 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;

SCl2; diisobutylaluminium hydride multistep reaction, various reducing agents, various solvents; Product distribution;

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