N-环己基-N,4-二甲基苯磺酰胺合成路线 (共 3 条)
反应条件
gallium; iodine
T=105°C; 24 h; Inert atmosphereneat (no solvent);
参考文献
Jaspers, Daniel; Kubiak, Raphael; Doye, Sven
Synlett, 2010 , # 8 art. no. G04710ST, p. 1268 - 1272
反应条件
1: With 2,4,6-trichloro-1,3,5-triazine in acetonitrile
T=20°C; 0.5 h;
2: With triethylamine in acetonitrile
参考文献
Rad, Mohammad Navid Soltani; Khalafi-Nezhad, Ali; Asrari, Zeinab; Behrouz, Somayeh; Amini, Zohreh; Behrouz, Marzieh
Synthesis, 2009 , # 23 art. no. Z15009SS, p. 3983 - 3988
反应条件
copper(l) iodide; di-tert-butyl peroxide; 4,7-Dimethoxy-1,10-phenanthroline in 1,2-dichloro-benzene
T=100°C; 24 h; Inert atmosphere;
参考文献
Tran, Ba L.; Li, Bijie; Driess, Matthias; Hartwig, John F.
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2555 - 2563