4-(3-硝基吡啶-2-基)哌嗪-1-甲酸叔丁酯合成路线 (共 3 条)
反应条件
acetic acid
T=130°C; 3 h; Reflux;
参考文献
EMS S.A.
Patent: US2012/115817 A1, 2012 ;
Location in patent: Page/Page column 41 ;
反应条件
1: hydrazine hydrate / methanol / 16 h / Reflux
2: acetic acid / 3 h / 130 °C / Reflux
View Scheme
参考文献
EMS S. A.; Universidade Estadual Paulista Julio De Mesquita Filho - UNESP
Patent: EP2418200 A1, 2012 ;
反应条件
1: Reflux
2: hydrazine hydrate / methanol / 16 h / Reflux
3: acetic acid / 3 h / 130 °C / Reflux
View Scheme
参考文献
EMS S. A.; Universidade Estadual Paulista Julio De Mesquita Filho - UNESP
Patent: EP2418200 A1, 2012 ;