乙酰溴-α-D-葡萄糖合成路线 （共 502 条）
反应条件
N(Et)4ClO4 in acetonitrile Elimination; Dimerization; Acetylation; Electrochemical reaction; Product distribution; Further Variations:different charge and supporting electrolyte;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 65, # 6 p. 881 - 898
反应条件
pyridine 1.) CH2Cl2, reflux, 8 h; other solvents, other reaction time, pyridine presence, 2.) room temperature, 24 h; other tetra-O-acetyl D-glucopyranosyl halides, other zinc salts of alcohols, phenols, thiols; Product distribution;
参考文献
Carbohydrate Research, , vol. 285, p. 159 - 165
反应条件
methanol; sodium methylate
参考文献
Hay; Haynes
Journal of the Chemical Society, 1958 , p. 2231,2232
反应条件
1: With potassium carbonate in dimethyl sulfoxide Koenigs-Knorr reaction; 2: With sodium methylate in methanol T=20°C; 0.333333 h;
参考文献
Murota, Kaeko; Mitsukuni, Yuki; Ichikawa, Mami; Tsushida, Tojiro; Miyamoto, Sayuri; Terao, Junji
Journal of agricultural and food chemistry, 2004 , vol. 52, # 7 p. 1907 - 1912
反应条件
water; silver carbonate in acetone 0.5 h;
参考文献
Sabesan; Neira
Carbohydrate Research, 1992 , vol. 223, p. 169 - 185
反应条件
AcrH(+)I(-); sodium cyanoborohydride in acetonitrile T=20°C; 240 h;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
sodium cyanoborohydride in nitromethane T=100°C; 10.5 h; Inert atmosphere;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
N,N,N',N'-tetramethyl-urea; silver trifluoromethanesulfonate in various solvent(s) T=25°C; 1.5 h; Yields of byproduct given;
参考文献
Takeo, Ken'ichi
Carbohydrate Research, 1980 , vol. 87, p. 147 - 152
反应条件
sodium cyanoborohydride in tert-butyl alcohol 0.5 h; UV-irradiation;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
反应条件
sodium cyanoborohydride in nitromethane T=100°C; 5 h; Inert atmosphere;
参考文献
Bruyere, Isabelle; Toth, Zoltan; Benyahia, Hamida; Xue, Jia Lu; Praly, Jean-Pierre
Tetrahedron, 2013 , vol. 69, # 46 p. 9656 - 9662
